反应条件
lithium in tetrahydrofuran; water O2-free atmosphere; Li (cuttings) and Me3SnCl in THF (25°C, 15 h), filtrate added to dibromobicyclooctadiene (THF, -78°C)(molar ratio 2.08), stirring (room temp.), poured into water, extn. (pentane), drying (Na2SO4); monitored by (1)H-NMR;
参考文献
Zeitschrift fuer Naturforschung, B: Chemical Sciences, , vol. 43, # 11 p. 1405 - 1415