反应条件
in tetrahydrofuran; toluene under Ar or N2; THF and toluene added to Co complex and Me3SnF; mixed; heated at 70°C for 21 h; volatiles removed under reduced pressure; dissolved in toluene-pentane; filtered through Celite; crystd. from filtrate at -45°C; additional crop of crystals obtained by crystn. from mother liquor; elem. anal.;
参考文献
Dugan, Thomas R.; Goldberg, Jonathan M.; Brennessel, William W.; Holland, Patrick L.
Organometallics, 2012 , vol. 31, # 4 p. 1349 - 1360