反应条件
in tetrahydrofuran byproducts: LiCl, 1,3-[P(O)(OEt2)2]2-4-tert-Bu-C6H3; (N2); soln. of Me3SnLi in THF added dropwise to soln. of tin compd. in THF at -40°C; soln. stirred at -40°C for 15 h; concd. (vac., -20°C); not isolated; NMR monitoring;
参考文献
Organometallics, , vol. 19, # 22 p. 4613 - 4623
