Zavgorodnii, V. S.; Zubova, T. P.; Simin, V. B.; Petrov, A. A.
Journal of General Chemistry USSR (English Translation), 1981 , vol. 51, p. 1765 - 1773
Zhurnal Obshchei Khimii, 1981 , vol. 51, p. 2048 - 2057
in tetrahydrofuran soln. of Sn-compound added to soln. of Ti-compound in hexane (-78°C), stirred, temp. raised to 0°C, soln. became dark-brown; solvent evapd. in vac., residue washed with pentane, dried; elem. anal., chromy.;
参考文献
Journal of General Chemistry USSR (English Translation), , vol. 60, p. 1729 - 1733
Zhurnal Obshchei Khimii, , vol. 60, p. 1937 - 1942
in tetrahydrofuran pentadienyllithium, from penta-1,4-diene and butyllithium, quenching with trimethyltin chloride at -70°C, the reaction mixt. pouring into satd. aq. NH4Cl soln., dilg. with H2O and extg. with pentane, hexamethylditin freezing out at -15°C; a mixture of isomers (E/Z=83.6:16.4) b.p. 50°C/10mm, identificated by elem. anal., NMR and mass spectra;
参考文献
Australian Journal of Chemistry, , vol. 37, p. 1863 - 1880
