in [3.3.1]nonane distannane and freshly pptd. Cu heating in nonane in a sealed tube for 40 h at 160°C, liquid fraction decanting off, solid washing with nonane, solvent removing from combined solns.; Me2SnO isolated as Me2SnCl2;
参考文献
Journal of Organometallic Chemistry, , vol. 264, # 1-2 p. 245 - 252
acetic acid in acetic acid Kinetics; stannane was added to AcOH in a NMR tube, mixt. was kept for 21 d, reaction followed by (1)H NMR spectroscopy; ca. 34percent of the substrate was consumed, rate const. for the initial 5-10percent reaction (first 2 d) when only Me3SnOAc was formed; not isolated, identified by (1)H NMR spectrum;
参考文献
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Journal of Organometallic Chemistry, 1985 , vol. 287, p. 7 - 24
Shi, Jun; Manolikakes, Georg; Yeh, Chien-Hung; Guerrero, Carlos A.; Shenvi, Ryan A.; Shigehisa, Hiroki; Baran, Phil S.
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