反应条件
2,2'-azo-bisisobutyronitrile in toluene byproducts: (4S,5S)-4,5-dibenhydryl-2,2-dimethyl-1,3-dioxolane, (E)-2-methyl-3-phenylpropenoic acid; under N2; diester in dry toluene treated with Me3SnH in presence of AIBNat 75°C for 24 h; solvent removed under reduced pressure; subjec ted to column chromy. (silica gel, hexane, hexane-Et2O 98:2, 95:5, Et2O);
参考文献
Organometallics, , vol. 27, # 4 p. 660 - 665
