4-甲氧基三氟甲烷磺酸苯酯合成路线 （共 120 条）
反应条件
caesium carbonate; tri-cyclo-hexyl-phosphine; palladium diacetate in tetrahydrofuran
Suzuki-Miyaura reaction; 48 h; Heating;
参考文献
Molander, Gary A.; Petrillo, Daniel E.; Landzberg, Nicole R.; Rohanna, John C.; Biolatto, Betina
Synlett, 2005 , # 11 art. no. Y00205ST, p. 1763 - 1766
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate; triethylamine in acetonitrile
0.0833333 h; Irradiation; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Olofsson, Kristofer; Larhed, Mats; Hallberg, Anders
Journal of Organic Chemistry, 1998 , vol. 63, # 15 p. 5076 - 5079
反应条件
1: benzyl bromide With zinc in tetrahydrofuran
T=0°C; 2 h;
2: 4-methoxyphenyl triflate With 1,1'-bis-(diphenylphosphino)ferrocene; tetra-(n-butyl)ammonium iodide; bis(dibenzylideneacetone) palladium in tetrahydrofuran; 1-methyl-pyrrolidin-2-one
T=60°C; 6 h; Further stages.;
参考文献
Piber, Michael; Jensen, Anne Eeg; Rottlaender, Mario; Knochel, Paul
Organic Letters, 1999 , vol. 1, # 9 p. 1323 - 1326
反应条件
dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; palladium diacetate; potassium phosphate in tetrahydrofuran
T=60°C; Suzuki-Miyaura reaction; 1 h;
参考文献
Flaherty, Alice; Trunkfield, Amy; Barton, William
Organic Letters, 2005 , vol. 7, # 22 p. 4975 - 4978
反应条件
caesium carbonate; triphenylphosphine; palladium diacetate in N,N-dimethyl-formamide
T=150°C; 20 h;
参考文献
Roger, Julien; Doucet, Henri
Organic and Biomolecular Chemistry, 2008 , vol. 6, # 1 p. 169 - 174
反应条件
1,3-bis-(diphenylphosphino)propane; N-ethyl-N,N-diisopropylamine; bis-triphenylphosphine-palladium(II) chloride in N,N-dimethyl-formamide
Heating;
参考文献
Martorell, Gabriel; Garcias, Xavier; Janura, Marcus; Saa, Jose M.
Journal of Organic Chemistry, 1998 , vol. 63, # 10 p. 3463 - 3467
反应条件
sodium t-butanolate; (SIPr)Pd(allyl)Cl in tetrahydrofuran
T=60°C; 1 h;
参考文献
Viciu, Mihai S.; Germaneau, Romain F.; Nolan, Steven P.
Organic Letters, 2002 , vol. 4, # 23 p. 4053 - 4055
反应条件
tetrabutyl ammonium fluoride; bis(dibenzylideneacetone)-palladium(0); 2-dicyclohexylphosphino-1,1'-biphenyl in tetrahydrofuran
6 h; Heating;
参考文献
Seganish, W. Michael; DeShong, Philip
Journal of Organic Chemistry, 2004 , vol. 69, # 4 p. 1137 - 1143
反应条件
palladium on activated charcoal in N,N-dimethyl-formamide
T=160 - 165°C; 15 h;
参考文献
Lai, Chi Wai; Kwong, Fuk Yee; Wang, Yanchun; Chan, Kin Shing
Tetrahedron Letters, 2001 , vol. 42, # 29 p. 4883 - 4885
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Wang, Yanchun; Lai, Chi Wai; Kwong, Fuk Yee; Jia, Wen; Chan, Kin Shing
Tetrahedron, 2004 , vol. 60, # 42 p. 9433 - 9439
反应条件
potassium fluoride; palladium diacetate; tri-cyclo-hexyl-phosphine in tetrahydrofuran
T=20°C; Suzuki cross-coupling; 6 h;
参考文献
Littke, Adam F.; Dai, Chaoyang; Fu, Gregory C.
Journal of the American Chemical Society, 2000 , vol. 122, # 17 p. 4020 - 4028
