4-甲氧基三氟甲烷磺酸苯酯合成路线 （共 120 条）
反应条件
(N,N'-diarylimidazol-2-ylidene)-based palladacycle; sodium t-butanolate in toluene T=70°C; 2 h;
参考文献
Viciu, Mihai S.; Kelly III, Roy A.; Stevens, Edwin D.; Naud, Frederic; Studer, Martin; Nolan, Steven P.
Organic Letters, 2003 , vol. 5, # 9 p. 1479 - 1482
反应条件
tetrabutyl-ammonium chloride; caesium carbonate; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene; tris(dibenzylideneacetone)dipalladium (0) in toluene T=120°C; 22 h;
参考文献
Cacchi, Sandro; Fabrizi, Giancarlo; Goggiamani, Antonella; Parisi, Luca M.; Bernini, Roberta
Journal of Organic Chemistry, 2004 , vol. 69, # 17 p. 5608 - 5614
反应条件
zinc; Ni-dppf in acetonitrile T=80°C; 10 h;
参考文献
Takagi, Kentaro; Sakakibara, Yasumasa
Chemistry Letters, 1989 , p. 1957 - 1958
反应条件
Cl2Ni(1,2-bis(diphenylphosphino)ethane); potassium iodide; zinc in tetrahydrofuran; N,N-dimethyl-formamide T=67°C; 4 h;
参考文献
Jutand, Anny; Mosleh, Adil
Journal of Organic Chemistry, 1997 , vol. 62, # 2 p. 261 - 274
反应条件
caesium carbonate; tri-cyclo-hexyl-phosphine; palladium diacetate in tetrahydrofuran Suzuki-Miyaura reaction; 38 h; Heating;
参考文献
Molander, Gary A.; Petrillo, Daniel E.; Landzberg, Nicole R.; Rohanna, John C.; Biolatto, Betina
Synlett, 2005 , # 11 art. no. Y00205ST, p. 1763 - 1766
反应条件
triethylamine; Pd(Ac2O)2-DPPP in N,N-dimethyl-formamide T=100°C; 5 h;
参考文献
Cabri, Walter; Candiani, Ilaria; Bedeschi, Angelo; Santi, Roberto
Journal of Organic Chemistry, 1990 , vol. 55, # 11 p. 3654 - 3655
反应条件
1,3-bis-(diphenylphosphino)propane; triethylamine; palladium diacetate in N,N-dimethyl-formamide T=60°C; 14 h;
参考文献
Larhed, Mats; Andersson, Carl-Magnus; Hallberg, Anders
Tetrahedron, 1994 , vol. 50, # 2 p. 285 - 304
反应条件
tetrakis(triphenylphosphine) palladium(0); cesium fluoride in 1,2-dichloro-ethane T=75°C; 6 h; Inert atmosphereSealed tube;
参考文献
Ramgren, Stephen D.; Garg, Neil K.
Organic Letters, 2014 , vol. 16, # 3 p. 824 - 827
反应条件
1: Et3N / 1,3-bis(diphenylphosphino)propane / Pd(OAc)2 / dimethylformamide / 1.5 h / 80 °C 2: 5percent HCl / 0.5 h View Scheme
参考文献
Gogsig, Thomas M.; Kleimark, Jonatan; Nilsson Lill, Sten O.; Korsager, Signe; Lindhardt, Anders T.; Norrby, Per-Ola; Skrydstrup, Troels
Journal of the American Chemical Society, 2012 , vol. 134, # 1 p. 443 - 452
反应条件
in toluene
T=120°C; 3 h; Inert atmosphere;
参考文献
Maimone, Thomas J.; Milner, Phillip J.; Kinzel, Tom; Zhang, Yong; Takase, Michael K.; Buchwald, Stephen L.
Journal of the American Chemical Society, 2011 , vol. 133, # 45 p. 18106 - 18109
