2-羟基-5-甲基-3-硝基苯乙酮合成路线 （共 5 条）
反应条件
nitric acid in acetic acid 2.5 h; Ambient temperature;
参考文献
Synthesis, , # 11 p. 940 - 942
反应条件
1: 85 percent / 1.) AlCl3 / 1.) 70 -> 80 deg C, 2 h, 2.) 120 deg C, 40 min 2: 90 percent / HNO3 (100percent) / acetic acid / 2.5 h / Ambient temperature View Scheme
参考文献
Synthesis, , # 11 p. 940 - 942
反应条件
hydrogen; palladium on activated charcoal in ethanol
参考文献
Ford; Knowles; Lunt; et al.
Journal of Medicinal Chemistry, 1986 , vol. 29, # 4 p. 538 - 549
反应条件
in benzene 6 h; Heating;
参考文献
Kalaiya; Parikh
Journal of the Indian Chemical Society, 1987 , vol. 64, # 3 p. 172 - 175
反应条件
1: 1-(2-hydroxy-5-methyl-3-nitro-phenyl)-ethanone With sodium ethanolate in ethanol
0.5 h;
2: oxalic acid diethyl ester in ethanol
Claisen condensation; 2 h; Heating;
参考文献
Anderluh, Marko; Marc, Gasper; Dolenc, Marija Sollner
Synthetic Communications, 2005 , vol. 35, # 11 p. 1461 - 1470
