1-脱氧-1-(苯基二硫代)-.beta.-D-吡喃葡萄糖四乙酸酯合成路线 （共 8 条）
反应条件
diethylazodicarboxylate in tetrahydrofuran
T=20°C; 3 h;
参考文献
Ribeiro Morais, Goreti; Falconer, Robert A.
Tetrahedron Letters, 2007 , vol. 48, # 43 p. 7637 - 7641
反应条件
in 1,2-dichloro-ethane
Reflux;
参考文献
Aversa, Maria Chiara; Barattucci, Anna; Bonaccorsi, Paola
European Journal of Organic Chemistry, 2009 , # 36 p. 6355 - 6359
反应条件
in dichloromethane
T=20°C; 0.75 h;
参考文献
Illyes, Tuende-Zita; Szabo, Tamas; Szilagyi, Laszlo
Carbohydrate Research, 2011 , vol. 346, # 12 p. 1622 - 1627
反应条件
in dichloromethane
T=20°C; 0.75 h;
参考文献
Illyes, Tuende-Zita; Szabo, Tamas; Szilagyi, Laszlo
Carbohydrate Research, 2011 , vol. 346, # 12 p. 1622 - 1627
反应条件
1: benzene
2: benzene
View Scheme
参考文献
Emde
Patent: DE804572 , 1949 ;
DRP/DRBP Org.Chem.
反应条件
1: 3-chloro-benzenecarboperoxoic acid
2: 1,2-dichloro-ethane / Reflux
View Scheme
参考文献
Aversa, Maria Chiara; Barattucci, Anna; Bonaccorsi, Paola
European Journal of Organic Chemistry, 2009 , # 36 p. 6355 - 6359
反应条件
1.1: silver(I) acetate / ethyl acetate / 0.67 h / 20 °C
1.2: 0.17 h / 0 - 20 °C
2.1: dichloromethane / 0.75 h / 20 °C
View Scheme
参考文献
Illyes, Tuende-Zita; Szabo, Tamas; Szilagyi, Laszlo
Carbohydrate Research, 2011 , vol. 346, # 12 p. 1622 - 1627
参考文献
Emde
Patent: DE804572 , 1949 ;
DRP/DRBP Org.Chem.
