1-甲基-1H-咪唑-4-甲腈合成路线 (共 9 条)
反应条件
in isobutyramide T=180°C; 0.75 h; Microwave irradiation;
参考文献
WO2009/70485 A1, ;
Page/Page column 117 ;
WO 2009/070485 A1
反应条件
T=210 - 220°C; 0.0833333 h;
参考文献
Subrayan, Ramachandran P.; Thurber, Ernest L.; Rasmussen, Paul G.
Tetrahedron, 1994 , vol. 50, # 9 p. 2641 - 2656
反应条件
in acetonitrile 10 h; Irradiation;
参考文献
Wakamatsu, Shigeru; Barltrop, John A.; Day, A. Colin
Chemistry Letters, 1982 , p. 667 - 670
反应条件
1: 87 percent / 40percent tetraethylammonium hydroxide / H2O / 0.5 h / Ambient temperature 2: 72 percent / 0.08 h / 210 - 220 °C View Scheme
参考文献
Tetrahedron, , vol. 50, # 9 p. 2641 - 2656
反应条件
in acetonitrile Irradiation;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 12 p. 604 - 606
反应条件
in methanol Ambient temperatureelectrooxidation at a platinum anode vs. SCE;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 60, # 10 p. 3693 - 3696
反应条件
in acetonitrile 2.5 h; Ambient temperatureIrradiation;
参考文献
Chemistry Letters, , p. 667 - 670
反应条件
in acetonitrile Irradiation;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 12 p. 604 - 606
反应条件
potassium fluoride on basic alumina T=20°C; 420768 h; Product distribution; Further Variations:ReagentsTemperatures;
参考文献
Journal of Heterocyclic Chemistry, , vol. 44, # 6 p. 1445 - 1451