2-(2-碘-四氟乙氧基)四氟乙基硫酰氟合成路线 （共 15 条）
反应条件
bromine; iodine in diethylene glycol dimethyl ether P=15001.2 Torr; 4 h;
参考文献
Bargigia, G. A.; Caporiccio, G.; Pianca, M.
Journal of Fluorine Chemistry, 1982 , vol. 19, p. 403 - 410
参考文献
Gmelin Handbook: F: PerFHalOrg.SVol.3, 6.2.3.4, page 152 - 186
反应条件
autoclave, 20°C, 5 h;
参考文献
DE2934194 , ;
C.A., , vol. 93, p. 7658
→
67990-76-51,1,2,2-四氟-2-(1,1,2,2,3,3,4,4-八氟-4-碘丁氧基)乙烷磺酰氯
参考文献
Bargigia, G. A.; Caporiccio, G.; Pianca, M.
Journal of Fluorine Chemistry, 1982 , vol. 19, p. 403 - 410
→
67990-76-51,1,2,2-四氟-2-(1,1,2,2,3,3,4,4-八氟-4-碘丁氧基)乙烷磺酰氯+
参考文献
Gmelin Handbook: F: PerFHalOrg.SVol.3, 6.2.3.4, page 152 - 186
反应条件
180°C, 6 h, 2 molecules of CF2CF2;
参考文献
Gmelin Handbook: F: PerFHalOrg.SVol.3, 6.2.3.4, page 152 - 186
反应条件
methanol; copper(l) iodide in N,N-dimethyl-formamide T=120°C; 8 h; Yield given. Yields of byproduct given;
参考文献
Long, Zheng-Yu; Duan, Jian-Xin; Lin, Yuan-Bin; Guo, Cai-Yun; Chen, Qing-Yun
Journal of Fluorine Chemistry, 1996 , vol. 78, # 2 p. 177 - 181
反应条件
copper(l) iodide in N,N-dimethyl-formamide T=120°C; 8 h; Yield given. Yields of byproduct given;
参考文献
Long, Zheng-Yu; Duan, Jian-Xin; Lin, Yuan-Bin; Guo, Cai-Yun; Chen, Qing-Yun
Journal of Fluorine Chemistry, 1996 , vol. 78, # 2 p. 177 - 181
反应条件
in tetrahydrofuran
155°C, 2 h;
参考文献
Gmelin Handbook: F: PerFHalOrg.SVol.3, 6.2.3.4, page 152 - 186
参考文献
Gmelin Handbook: F: PerFHalOrg.SVol.3, 6.2.3.4, page 152 - 186
