5-(3-甲基苯基)-1,3,4-噁二唑-2-硫醇合成路线 (共 7 条)
反应条件
in N,N-dimethyl-formamide 0.00833333 h; Irradiation;
参考文献
Joshi, Sachin; Karnik
Synthetic Communications, 2002 , vol. 32, # 1 p. 111 - 114
反应条件
1: KOH 2: Heating View Scheme
参考文献
Heterocycles, , vol. 20, # 11 p. 2211 - 2224
反应条件
potassium hydroxide in ethanol Heating;
参考文献
Journal of the Chinese Chemical Society, , vol. 52, # 3 p. 539 - 544
反应条件
1: thionyl chloride / 5 h / |Reflux 2: triethylamine / dichloromethane / 0 °C 3: hydrazine hydrate / methanol / 5 h / |Reflux 4: potassium hydroxide / methanol / 20 °C / |Reflux 5: hydrogenchloride / water / 0 - 5 °C View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 24, # 1 p. 192 - 194
反应条件
1: triethylamine / dichloromethane / 0 °C 2: hydrazine hydrate / methanol / 5 h / |Reflux 3: potassium hydroxide / methanol / 20 °C / |Reflux 4: hydrogenchloride / water / 0 - 5 °C View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 24, # 1 p. 192 - 194
反应条件
1: hydrazine hydrate / methanol / 5 h / |Reflux 2: potassium hydroxide / methanol / 20 °C / |Reflux 3: hydrogenchloride / water / 0 - 5 °C View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 24, # 1 p. 192 - 194
反应条件
hydrazine hydrate 4 h; Heating;
参考文献
Joshi; Karnik
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2006 , vol. 45, # 4 p. 1057 - 1059