5-(4-甲氧苯基)乙内酰脲合成路线 (共 14 条)
反应条件
1: 86 percent / 10percent aq. NaOH / 24 h / Heating 2: 63.2 percent / 4N NaOH / 0.33 h / Ambient temperature View Scheme
参考文献
Pinna, G. A.; Gavini, E.; Cignarella, G.; Scolastico, S.; Fadda, P.
European Journal of Medicinal Chemistry, 1995 , vol. 30, # 6 p. 515 - 520
反应条件
iron(II,III) oxide in neat (no solvent)
T=70°C; Bucherer-Bergs Reaction; 0.383333 h;
参考文献
Safari, Javad; Javadian, Leila
Comptes Rendus Chimie, 2013 , vol. 16, # 12 p. 1165 - 1171
反应条件
anhydrous magnesium perchlorate in 1,4-dioxane
T=40°C; 21 h;
参考文献
Cativiela, Carlos; Fraile, Jose M.; Garcia, Jose I.; Lafuente, Gustavo; Mayoral, Jose A.; Tahir, Rachid; Pallares, Antonio
Journal of Catalysis, 2004 , vol. 226, # 1 p. 192 - 196
反应条件
in ethanol; water
T=60°C; 12 h;
参考文献
Pinna, G. A.; Gavini, E.; Cignarella, G.; Scolastico, S.; Fadda, P.
European Journal of Medicinal Chemistry, 1995 , vol. 30, # 6 p. 515 - 520
参考文献
Coghill; Johnson
Journal of the American Chemical Society, 1925 , vol. 47, p. 191
反应条件
Erwaermen des Reaktionsprodukts mit Salzsaeure;
参考文献
Coghill; Johnson
Journal of the American Chemical Society, 1925 , vol. 47, p. 191
反应条件
in ethanol; water
T=45°C; 4 h; ultrasonication: other reaction conditions (particularly, absence of ultrasonication); Product distribution;
参考文献
Li, Jital; Li, Lijun; Li, Tongshuang; Waog, Jianzhong
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1998 , vol. 37, # 3 p. 298 - 300
反应条件
potassium hydroxide
beim nachfolgenden Ansaeuern;
参考文献
Clarke; Francis
Journal of the Chemical Society, 1911 , vol. 99, p. 323
反应条件
1: ammonia; KOH-solution
2: phenylhydrazine; benzene
3: natrium carbonate
4: alcoholic KOH-solution / beim nachfolgenden Ansaeuern
View Scheme
参考文献
Clarke; Francis
Journal of the Chemical Society, 1911 , vol. 99, p. 323
反应条件
1: natrium carbonate
2: alcoholic KOH-solution / beim nachfolgenden Ansaeuern
View Scheme
参考文献
Clarke; Francis
Journal of the Chemical Society, 1911 , vol. 99, p. 323