甲基-6-O-对甲苯磺酰基-Alpha-D-葡萄糖苷合成路线 （共 15 条）
反应条件
1: 89 percent / hexamethyldisilazane, pyridine / 1.) 0 deg C, 15 min, 2.) r.t., 1 h 2: LiPPh2 / tetrahydrofuran / 1 h / 0 - 10 °C View Scheme
参考文献
Dahlhoff, Wilhelm V.; Radkowski, Karin
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 1996 , vol. 51, # 6 p. 891 - 896
参考文献
Griffith, Byron R.; Krepel, Candace; Fu, Xun; Blanchard, Sophie; Ahmed, Aqeel; Edmiston, Charles E.; Thorson, Jon S.
Journal of the American Chemical Society, 2007 , vol. 129, # 26 p. 8150 - 8155
反应条件
pyridine
48 h; Ambient temperature;
参考文献
Dahlhoff, Wilhelm V.; Radkowski, Karin
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 1996 , vol. 51, # 6 p. 891 - 896
反应条件
1: pyridine
2: methanol; ammonia
View Scheme
参考文献
Helferich; Becker
Justus Liebigs Annalen der Chemie, 1924 , vol. 440, p. 1,12
参考文献
Haworth et al.
Journal of the Chemical Society, 1941 , p. 88,97
Full Text Show Details
Helferich; Himmen
Chemische Berichte, 1928 , vol. 61, p. 1825,1833
Chemische Berichte, 1929 , vol. 62, p. 2136,2138
反应条件
1: pyridine
2: methanol; sodium
View Scheme
参考文献
Haworth et al.
Journal of the Chemical Society, 1941 , p. 88,97
Full Text Show Details
Helferich; Himmen
Chemische Berichte, 1928 , vol. 61, p. 1825,1833
Chemische Berichte, 1929 , vol. 62, p. 2136,2138
参考文献
Helferich; Becker
Justus Liebigs Annalen der Chemie, 1924 , vol. 440, p. 1,12
反应条件
1: pyridine
2: methanol; ammonia
View Scheme
参考文献
Helferich; Becker
Justus Liebigs Annalen der Chemie, 1924 , vol. 440, p. 1,12
反应条件
1: chloroform; hydrogen chloride
2: pyridine
3: methanol; ammonia
View Scheme
参考文献
Helferich; Becker
Justus Liebigs Annalen der Chemie, 1924 , vol. 440, p. 1,12
反应条件
4-(N,N-dimethlyamino)pyridine; di(n-butyl)tin oxide
1.) MeOH, reflux, 3-10 h 2.) dioxane, room temp., 11 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Tsuda; Nishimura; Kobayashi; Sato; Kanemitsu
Chemical and Pharmaceutical Bulletin, 1991 , vol. 39, # 11 p. 2883 - 2887
