1: ethyl (2Z)-3-iodo-3-phenylprop-2-enoate With iso-propylmagnesium bromide in tetrahydrofuran
T=-20°C; 0.5 h;
2: benzaldehyde in tetrahydrofuran
T=-40 - -20°C; Further stages.;
参考文献
Sapountzis; Dohle; Knochel
Chemical Communications, 2001 , # 20 p. 2068 - 2069
T=135 - 640°C; P=0.1 Torr; 0.75 h; Further byproducts given;
参考文献
Brown, Roger F. C.; Eastwood, Frank W.; Chaichit, Narongsak; Gatehouse, Bryan M.; Pfeiffer, Jan M.; Woodroffe, David
Australian Journal of Chemistry, 1981 , vol. 34, # 7 p. 1467 - 1481
