乙基6,7-二甲氧基-3-甲基-4-氧代-1-(3,4,5-三甲氧基苯基)-1,2,3,4-四氢-2-萘l烯羧酸酯合成路线 （共 20 条）
反应条件
sodium nitrite; trichloroacetic acid; Copper(I)chloride in benzene
参考文献
Biaschim S.p.A.
Patent: US4542233 A1, 1985 ;
反应条件
sulfuric acid 3 h; Heating;
参考文献
Terao, Yosuke; Ijima, Yoichiro; Kakidani, Hitoshi; Ohta, Hiromichi
Bulletin of the Chemical Society of Japan, 2003 , vol. 76, # 12 p. 2395 - 2397
反应条件
potassium phosphate; Ni(PCy3)2Cl2 in toluene T=130°C; Suzuki-Miyaura Coupling;
参考文献
US2011/77406 A1, ;
Page/Page column 9-10; sheet 14/14 ;
反应条件
potassium phosphate; Ni(PCy3)2Cl2 in toluene T=130°C; Suzuki-Miyaura coupling reaction; 24 h; Inert atmosphere;
参考文献
Journal of the American Chemical Society, , vol. 131, # 49 p. 17748 - 17749
反应条件
sulfuric acid in methanol
反应条件
lead(IV) acetate; perchloric acid in water 48 h; Ambient temperature;
参考文献
Pol; Sudalai; Sonawane
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 1998 , vol. 37, # 3 p. 239 - 246
参考文献
Wuts, Peter G. M.; Bergh, Carol L.
Tetrahedron Letters, 1986 , vol. 27, # 34 p. 3995 - 3998
反应条件
1.1: sodium hydroxide; silver trifluoromethanesulfonate / methanol / 0 °C 1.2: Molecular sieve 2.1: iodine; silver trifluoromethanesulfonate / chloroform / 65 °C 3.1: manganese; trifluoroacetic acid / NiBr2bipy / N,N-dimethyl-formamide / 50 °C 4.1: potassium phosphate / Ni(PCy3)2Cl2 / toluene / 130 °C View Scheme
反应条件
1: iodine; silver trifluoromethanesulfonate / chloroform / 65 °C 2: manganese; trifluoroacetic acid / NiBr2bipy / N,N-dimethyl-formamide / 50 °C 3: potassium phosphate / Ni(PCy3)2Cl2 / toluene / 130 °C View Scheme
反应条件
1: manganese; trifluoroacetic acid / NiBr2bipy / N,N-dimethyl-formamide / 50 °C 2: potassium phosphate / Ni(PCy3)2Cl2 / toluene / 130 °C View Scheme
