乙基6,7-二甲氧基-3-甲基-4-氧代-1-(3,4,5-三甲氧基苯基)-1,2,3,4-四氢-2-萘l烯羧酸酯合成路线 （共 20 条）
反应条件
tetrakis(triphenylphosphine) palladium(0); phosphate potassium salt in 1,4-dioxane T=100°C; Suzuki-Miyaura coupling; 3 h; Inert atmosphere;
参考文献
Advanced Synthesis and Catalysis, , vol. 354, # 4 p. 751 - 756
反应条件
1: NaHSO3 / methanol; H2O 2: DMSO, Ac2O / 24 h / Ambient temperature 3: 90 percent / methanol View Scheme
参考文献
Tetrahedron Letters, , vol. 27, # 34 p. 3995 - 3998
反应条件
1: DMSO, Ac2O / 24 h / Ambient temperature 2: 90 percent / methanol View Scheme
参考文献
Tetrahedron Letters, , vol. 27, # 34 p. 3995 - 3998
反应条件
1: hydrogen 2: diisopropylamine / dichloromethane / -15 - 20 °C 3: tetrakis(triphenylphosphine) palladium(0); phosphate potassium salt / 1,4-dioxane / 3 h / 100 °C / Inert atmosphere View Scheme
参考文献
Advanced Synthesis and Catalysis, , vol. 354, # 4 p. 751 - 756
反应条件
1: sulfuric acid 2: potassium carbonate / N,N-dimethyl-formamide / 70 °C / Inert atmosphere 3: hydrogen 4: diisopropylamine / dichloromethane / -15 - 20 °C 5: tetrakis(triphenylphosphine) palladium(0); phosphate potassium salt / 1,4-dioxane / 3 h / 100 °C / Inert atmosphere View Scheme
参考文献
Advanced Synthesis and Catalysis, , vol. 354, # 4 p. 751 - 756
反应条件
1: potassium carbonate / N,N-dimethyl-formamide / 70 °C / Inert atmosphere 2: hydrogen 3: diisopropylamine / dichloromethane / -15 - 20 °C 4: tetrakis(triphenylphosphine) palladium(0); phosphate potassium salt / 1,4-dioxane / 3 h / 100 °C / Inert atmosphere View Scheme
参考文献
Advanced Synthesis and Catalysis, , vol. 354, # 4 p. 751 - 756
反应条件
1: diisopropylamine / dichloromethane / -15 - 20 °C 2: tetrakis(triphenylphosphine) palladium(0); phosphate potassium salt / 1,4-dioxane / 3 h / 100 °C / Inert atmosphere View Scheme
参考文献
Advanced Synthesis and Catalysis, , vol. 354, # 4 p. 751 - 756
反应条件
n-butyllithium; tris(dibenzylideneacetone)dipalladium (0); tri-isopropoxy-borane; sodium carbonate; triphenylphosphine Multistep reaction;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 9, # 3 p. 307 - 312
反应条件
sulfuric acid in 1,4-dioxane 2 h; Heating;
参考文献
Morrone; Nicolosi; Patti; Piattelli
Tetrahedron Asymmetry, 1995 , vol. 6, # 7 p. 1773 - 1778
反应条件
sulfuric acid in 1,4-dioxane 2 h; Heating;
参考文献
Morrone; Nicolosi; Patti; Piattelli
Tetrahedron Asymmetry, 1995 , vol. 6, # 7 p. 1773 - 1778
