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乙二醇
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63148-62-9
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二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
66203-04-1
合成路线
（共 6 条）
109-01-3
N-甲基哌嗪
+
66203-90-5
→
反应条件
66203-04-1
反应条件
potassium carbonate; sodium iodide in acetonitrile 15 h; Heating;
参考文献
Bourgery, Guy; Dostert, Philippe; Lacour, Alain; Langlois, Michel; Pourrias, Bernard; Tisne-Versailles, Jacky
Journal of Medicinal Chemistry, 1981 , vol. 24, # 2 p. 159 - 167
52631-79-5
→
反应条件
66203-04-1
反应条件
1: 90 percent / HCl / ethanol / 20 h / Heating 2: 89 percent / CHCl3 / 2 h / Ambient temperature 3: 62 percent / K2CO3 / acetonitrile / 4.5 h / Heating 4: 80 percent / NaI, K2CO3 / acetonitrile / 15 h / Heating View Scheme
参考文献
Bourgery, Guy; Dostert, Philippe; Lacour, Alain; Langlois, Michel; Pourrias, Bernard; Tisne-Versailles, Jacky
Journal of Medicinal Chemistry, 1981 , vol. 24, # 2 p. 159 - 167
484-51-5
凯林酮
→
反应条件
66203-04-1
反应条件
1: 82 percent / hydroxylamine hydrochloride, conc. NaOH / ethanol; H2O / 6 h / Heating 2: 75 percent / aq. AcOH, HCl(g) / 0.5 h / 90 °C 3: 90 percent / HCl / ethanol / 20 h / Heating 4: 89 percent / CHCl3 / 2 h / Ambient temperature 5: 62 percent / K2CO3 / acetonitrile / 4.5 h / Heating 6: 80 percent / NaI, K2CO3 / acetonitrile / 15 h / Heating View Scheme
参考文献
Bourgery, Guy; Dostert, Philippe; Lacour, Alain; Langlois, Michel; Pourrias, Bernard; Tisne-Versailles, Jacky
Journal of Medicinal Chemistry, 1981 , vol. 24, # 2 p. 159 - 167
52631-78-4
→
反应条件
66203-04-1
反应条件
1: 75 percent / aq. AcOH, HCl(g) / 0.5 h / 90 °C 2: 90 percent / HCl / ethanol / 20 h / Heating 3: 89 percent / CHCl3 / 2 h / Ambient temperature 4: 62 percent / K2CO3 / acetonitrile / 4.5 h / Heating 5: 80 percent / NaI, K2CO3 / acetonitrile / 15 h / Heating View Scheme
参考文献
Bourgery, Guy; Dostert, Philippe; Lacour, Alain; Langlois, Michel; Pourrias, Bernard; Tisne-Versailles, Jacky
Journal of Medicinal Chemistry, 1981 , vol. 24, # 2 p. 159 - 167
52631-80-8
→
反应条件
66203-04-1
反应条件
1: 89 percent / CHCl3 / 2 h / Ambient temperature 2: 62 percent / K2CO3 / acetonitrile / 4.5 h / Heating 3: 80 percent / NaI, K2CO3 / acetonitrile / 15 h / Heating View Scheme
参考文献
Bourgery, Guy; Dostert, Philippe; Lacour, Alain; Langlois, Michel; Pourrias, Bernard; Tisne-Versailles, Jacky
Journal of Medicinal Chemistry, 1981 , vol. 24, # 2 p. 159 - 167
66203-89-2
→
反应条件
66203-04-1
反应条件
1: 62 percent / K2CO3 / acetonitrile / 4.5 h / Heating 2: 80 percent / NaI, K2CO3 / acetonitrile / 15 h / Heating View Scheme
参考文献
Bourgery, Guy; Dostert, Philippe; Lacour, Alain; Langlois, Michel; Pourrias, Bernard; Tisne-Versailles, Jacky
Journal of Medicinal Chemistry, 1981 , vol. 24, # 2 p. 159 - 167
