N-苯甲氧基甲酰基-1,2,5,6-四氢吡啶合成路线 （共 25 条）
反应条件
1: triethylamine / dichloromethane / 0 °C 2: potassium carbonate / N,N-dimethyl-formamide / 10 - 80 °C View Scheme
参考文献
Synthesis, , # 22 art. no. Z72611SS, p. 3669 - 3674
反应条件
1: triethylamine 2: triethylamine / dichloromethane / 0 °C 3: potassium carbonate / N,N-dimethyl-formamide / 10 - 80 °C View Scheme
参考文献
Synthesis, , # 22 art. no. Z72611SS, p. 3669 - 3674
反应条件
1: triethylamine 2: triethylamine / dichloromethane / 0 °C 3: potassium carbonate / N,N-dimethyl-formamide / 10 - 80 °C View Scheme
参考文献
Synthesis, , # 22 art. no. Z72611SS, p. 3669 - 3674
反应条件
1: triethylamine 2: triethylamine / dichloromethane / 0 °C 3: potassium carbonate / N,N-dimethyl-formamide / 10 - 80 °C View Scheme
参考文献
Synthesis, , # 22 art. no. Z72611SS, p. 3669 - 3674
反应条件
1: triethylamine / dichloromethane / 0 °C 2: potassium carbonate / N,N-dimethyl-formamide / 10 - 80 °C View Scheme
参考文献
Synthesis, , # 22 art. no. Z72611SS, p. 3669 - 3674
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; tetrakis(triphenylphosphine) palladium(0); cyclohexa-1,4-diene; α,α,α-trifluorotoluene; N,N-dicyclohexylmethylamine T=110°C; Heck Reaction; 12 h; Inert atmosphereGlovebox; Mechanism;
参考文献
Chemical Communications, , vol. 50, # 28 p. 3725 - 3728
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; tetrakis(triphenylphosphine) palladium(0); cyclohexa-1,4-diene; α,α,α-trifluorotoluene; N,N-dicyclohexylmethylamine T=110°C; Heck Reaction; 12 h; Inert atmosphereGlovebox; Mechanism;
参考文献
Chemical Communications, , vol. 50, # 28 p. 3725 - 3728
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; tetrakis(triphenylphosphine) palladium(0); α,α,α-trifluorotoluene; N,N-dicyclohexylmethylamine T=110°C; Heck Reaction; 12 h; Inert atmosphereGlovebox; Mechanism;
参考文献
Zou, Yinjun; Zhou, Jianrong
Chemical Communications, 2014 , vol. 50, # 28 p. 3725 - 3728
反应条件
sodium hydroxide; dihydrogen peroxide; bis-(1,2-dimethylpropyl)borane 1.) THF, 25 deg C, 1 h, 2.) 25 deg C, 6 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Brown, Herbert C.; Prasad, J. V. N. Vara; Zee, Sheng-Hsu
Journal of Organic Chemistry, 1985 , vol. 50, # 10 p. 1582 - 1589
反应条件
sodium hydroxide; dihydrogen peroxide; bis-(1,2-dimethylpropyl)borane 1.) THF, 25 deg C, 1 h, 2.) 25 deg C, 6 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Brown, Herbert C.; Prasad, J. V. N. Vara; Zee, Sheng-Hsu
Journal of Organic Chemistry, 1985 , vol. 50, # 10 p. 1582 - 1589
