4-甲氧基-2,4,6-环庚三烯-1-酮合成路线 （共 17 条）
反应条件
aluminum oxide in chloroform
2 h;
参考文献
Yagihara, Morio; Kitahara, Yoshio; Asao, Toyonobu
Bulletin of the Chemical Society of Japan, 1980 , vol. 53, # 1 p. 236 - 238
反应条件
selenium(IV) oxide in tert-butyl alcohol
0.166667 h; Heating;
参考文献
Cavazza, Marino; Pietra, Francesco
Journal of the Chemical Society, Chemical Communications, 1986 , # 19 p. 1480 - 1481
参考文献
Chapman,O.L.; Fitton,P.
Journal of the American Chemical Society, 1961 , vol. 83, p. 1005 - 1006
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Chapman,O.L.; Fitton,P.
Journal of the American Chemical Society, 1963 , vol. 85, p. 41 - 47
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Coffey; Johnson
Journal of the Chemical Society, 1958 , p. 1741,1743
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Nozoe et al.
Chemistry and Industry (London, United Kingdom), 1955 , p. 66
反应条件
1: 34.4 percent / triethylamine / CH2Cl2 / 25 h / Heating
2: 58 percent / alumina / CHCl3 / 2 h
View Scheme
参考文献
Yagihara, Morio; Kitahara, Yoshio; Asao, Toyonobu
Bulletin of the Chemical Society of Japan, 1980 , vol. 53, # 1 p. 236 - 238
反应条件
1: 83 percent / MeONa / -10 - 0 °C / anodic oxidation
View Scheme
参考文献
Shono, Tatsuya; Nozoe, Tetsuo; Maekawa, Hirofumi; Kashimura, Shigenori
Tetrahedron Letters, 1988 , vol. 29, # 5 p. 555 - 558
反应条件
1: 98 percent / Heating
2: 83 percent / MeONa / -10 - 0 °C / anodic oxidation
View Scheme
参考文献
Shono, Tatsuya; Nozoe, Tetsuo; Maekawa, Hirofumi; Kashimura, Shigenori
Tetrahedron Letters, 1988 , vol. 29, # 5 p. 555 - 558
反应条件
1: acetonitrile / 8 h / 0 °C / Irradiation
2: 38 percent / SeO2 / 2-methyl-propan-2-ol / 0.17 h / Heating
View Scheme
参考文献
Cavazza, Marino; Pietra, Francesco
Journal of the Chemical Society, Chemical Communications, 1986 , # 19 p. 1480 - 1481
参考文献
Chapman,O.L.; Fitton,P.
Journal of the American Chemical Society, 1963 , vol. 85, p. 41 - 47
反应条件
1: 85 percent / MeONa / -10 - 0 °C / anodic oxidation
View Scheme
参考文献
Shono, Tatsuya; Nozoe, Tetsuo; Maekawa, Hirofumi; Kashimura, Shigenori
Tetrahedron Letters, 1988 , vol. 29, # 5 p. 555 - 558
反应条件
1: 71 percent / Et4NOTs, NaOMe / -10 - 0 °C / carbon rod electrodes, 5 A, 3F/mol
2: 98 percent / 1 h / 150 °C
3: 83 percent / Et4NOTs, NaOMe / -10 - 0 °C / carbon rod electrodes, 5 A, 2.5 F/mol
View Scheme
参考文献
Shono, Tatsuya; Nozoe, Tetsuo; Maekawa, Hirofumi; Yamaguchi, Yoshihide; Kanetaka, Shinya; Masuda, Haruhisa; Okada, Toshio; Kashimura, Shigenori
Tetrahedron, 1991 , vol. 47, # 4-5 p. 593 - 603
