(4-氯苯基)-氨基甲酸苄酯合成路线 （共 5 条）
反应条件
potassium carbonate in tetrahydrofuran
T=20°C; 2 h; Inert atmosphere;
参考文献
Yang, Bo; Shi, Luyan; Wu, Jingjing; Fang, Xiang; Yang, Xueyan; Wu, Fanhong
Tetrahedron, 2013 , vol. 69, # 15 p. 3331 - 3337
反应条件
1: in tetrahydrofuran
T=55°C; 8 h; Inert atmosphere;
2: With water; ammonium chloride in tetrahydrofuran
Inert atmosphere;
参考文献
Yang, Haoran; Huang, Danfeng; Wang, Ke-Hu; Xu, Changming; Niu, Teng; Hu, Yulai
Tetrahedron, 2013 , vol. 69, # 12 p. 2588 - 2593
反应条件
ammonium hydroxide; iron in methanol
T=25°C; Reduction; condensation; 1 h; sonication;
参考文献
Chandrasekhar; Narsihmulu
Tetrahedron Letters, 2000 , vol. 41, # 41 p. 7969 - 7972
反应条件
in acetonitrile
16 h; Inert atmosphereReflux;
参考文献
Dube, Pascal; Fine Nathel, Noah F.; Vetelino, Michael; Couturier, Michel; Aboussafy, Claude Larrivee; Pichette, Simon; Jorgensen, Matthew L.; Hardink, Mark
Organic Letters, 2009 , vol. 11, # 24 p. 5622 - 5625
反应条件
1.1: ethylene dibromide / tetrahydrofuran / |Inert atmosphere; |Heating
1.2: 0.25 h / 20 °C / |Inert atmosphere
1.3: 20 °C / |Inert atmosphere
2.1: tetrahydrofuran / 8 h / 55 °C / |Inert atmosphere
2.2: |Inert atmosphere
View Scheme
参考文献
Yang, Haoran; Huang, Danfeng; Wang, Ke-Hu; Xu, Changming; Niu, Teng; Hu, Yulai
Tetrahedron, 2013 , vol. 69, # 12 p. 2588 - 2593
