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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
66224-66-6
合成路线
（共 291 条）
66224-66-6
→
反应条件
89419-12-5
反应条件
1: 30 percent / 1,1,1,3.3.3-hexamethyldisilazane, ammonium sulfate, mercuric cyanide / benzene / Heating 2: 77 percent / palladium oxide, cyclohexene / ethanol / 1.) 18 h; 2.) reflux, 2.5 h 3: 53 percent / triphenylphosphine, lithium azide, carbon tetrabromide / dimethylformamide / 24 h / Ambient temperature 4: 52 percent / 5percent Pd/C, H2 / aq. ethanol / 2 h / Ambient temperature View Scheme
参考文献
Ogilvie; Nguyen-Ba; Gillen; et al.
Canadian Journal of Chemistry, 1984 , vol. 62, # 2 p. 241 - 252
66224-66-6
→
反应条件
89760-72-5
反应条件
1: 40 percent / K2CO3 / dimethylsulfoxide / 120 h / Ambient temperature 2: 1) HCO2H; 2) aq. H2O2; 3) KOH / 1) H2O, 70-80 deg C, 10 min; 2) H2O, 25 deg C, 15 h; 3) H2O, 95 deg C, 10 min View Scheme
参考文献
Roveri; Cavrini; Gatti; et al.
European Journal of Medicinal Chemistry, 1983 , vol. 18, # 6 p. 555 - 557
50563-72-9
2-(烯丙氧基)乙基 4-甲基苯磺酸盐
+
66224-66-6
→
反应条件
89760-73-6
反应条件
1: 6-aminopurine With potassium carbonate in N,N-dimethyl-formamide Heating; 2: 2-(allyloxy)ethyl tosylate in N,N-dimethyl-formamide Heating;
参考文献
Petrov; Ozerov; Novikov; Pannecouque; Balzarini; De Clercq
Chemistry of Heterocyclic Compounds, 2003 , vol. 39, # 9 p. 1218 - 1226
106-92-3
烯丙基缩水甘油醚
+
66224-66-6
→
反应条件
89760-74-7
反应条件
potassium carbonate in dimethyl sulfoxide 120 h; Ambient temperature;
参考文献
Roveri; Cavrini; Gatti; et al.
European Journal of Medicinal Chemistry, 1983 , vol. 18, # 6 p. 555 - 557
66224-66-6
→
反应条件
90973-36-7
反应条件
1: K2CO3 / dimethylformamide / 60 °C 2: aq. NaOH / methanol / 20 °C View Scheme
参考文献
Hisatome, Masao; Maruyama, Noriaki; Ikeda, Koichi; Furutera, Tetsuo; Ishikawa, Tomiyasu; Yamakawa, Koji
Chemical and Pharmaceutical Bulletin, 1996 , vol. 44, # 10 p. 1801 - 1811
66224-66-6
→
反应条件
918795-49-0
反应条件
1: 70 percent / dimethylformamide / 1 h / Heating 2: 38 percent / NaH / dimethylformamide / 16 h / 20 °C 3: 52 percent / sodium borohydride / methanol / 11 h / -5 - 0 °C 4: pyridine; DMAP / 48 h / 20 °C 5: 0.3 g / aq. NaOH / methanol / 48 h / 20 °C View Scheme
参考文献
Kotian, Pravin L.; Kumar, V. Satish; Lin, Tsu-Hsing; El-Kattan, Yahya; Ghosh, Ajit; Wu, Minwan; Cheng, Xiaogang; Bantia, Shanta; Babu, Yarlagadda S.; Chand, Pooran
Nucleosides, Nucleotides and Nucleic Acids, 2006 , vol. 25, # 2 p. 121 - 140
66224-66-6
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反应条件
919512-63-3
反应条件
1.1: NaH / dimethylformamide / 1 h / 60 °C 1.2: dimethylformamide / 16 h / 60 °C 2.1: 5.87 g / NH3 / methanol / 14 h / 20 °C 3.1: sodium tert-butoxide / dimethylformamide / 0.67 h / 20 °C 3.2: 27 percent / dimethylformamide / 72 h / 20 °C 4.1: 78 percent / TMSCl; LiAlH4 / tetrahydrofuran / -50 - 20 °C View Scheme
参考文献
Barral, Karine; Priet, Stephane; Sire, Josephine; Neyts, Johan; Balzarini, Jan; Canard, Bruno; Alvarez, Karine
Journal of Medicinal Chemistry, 2006 , vol. 49, # 26 p. 7799 - 7806
50-00-0
甲醛
+
66224-66-6
→
反应条件
95121-23-6
反应条件
sodium hydroxide in water T=20°C;
参考文献
Lang; Magnin; Mathis; Burger; Biellmann
Journal of Organic Chemistry, 2000 , vol. 65, # 23 p. 7825 - 7832
3970-21-6
2-甲氧基乙氧基甲基氯
+
66224-66-6
→
反应条件
95121-23-6
反应条件
sodium hydroxide in water Substitution; hydrolysis;
参考文献
Lang; Magnin; Mathis; Burger; Biellmann
Journal of Organic Chemistry, 2000 , vol. 65, # 23 p. 7825 - 7832
50-00-0
甲醛
+
66224-66-6
→
反应条件
95121-23-6
反应条件
in dimethylsulfoxide-d6; water T=40°C; detection of different reaction products at different reaction times; Product distribution;
参考文献
Botlan, D. J. Le
Magnetic Resonance in Chemistry, 1989 , vol. 27, # 3 p. 295 - 298
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