反式-6-甲基-3-庚烯合成路线 (共 12 条)
反应条件
aluminum oxide
T=385°C;
参考文献
Henne; Matuszak
Journal of the American Chemical Society, 1944 , vol. 66, p. 1651
反应条件
Cr2O3-catalyst
T=400°C; im Rohr;
参考文献
Komarewsky; Smith
Journal of the American Chemical Society, 1944 , vol. 66, p. 1117
反应条件
(TPP)Zr(O2tBu)2 in benzene
T=0°C; 72 h; Yield given. Yields of byproduct given;
参考文献
Shibata, Kenji; Aida, Takuzo; Inoue, Shohei
Tetrahedron Letters, 1992 , vol. 33, # 8 p. 1077 - 1080
反应条件
1: CH2Cl2 / -78 °C
2: 1) NaBH4, 2) PH3P / 1) i-PrOH, rt, 2) reflux
View Scheme
参考文献
Dybowski, Piotr; Skowronska, Aleksandra
Tetrahedron Letters, 1991 , vol. 32, # 34 p. 4385 - 4388
反应条件
sodium tetrahydroborate in methanol
Heating; Yield given. Yields of byproduct given;
参考文献
Dybowski, Piotr; Skowronska, Aleksandra
Tetrahedron Letters, 1991 , vol. 32, # 34 p. 4385 - 4388
反应条件
sodium tetrahydroborate; triphenylphosphine
1) i-PrOH, rt, 2) reflux; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Dybowski, Piotr; Skowronska, Aleksandra
Tetrahedron Letters, 1991 , vol. 32, # 34 p. 4385 - 4388
参考文献
Tuot
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1940 , vol. 211, p. 561
反应条件
lithium
1) ether, THF, -60 deg C, 2) -60 deg C, 8 h; Yield given. Multistep reaction;
参考文献
Barluenga, Jose; Yus, Miguel; Concellon, Jose M.; Bernad, Pablo
Journal of Chemical Research, Miniprint, 1980 , # 2 p. 677 - 692
参考文献
Henne; Matuszak
Journal of the American Chemical Society, 1944 , vol. 66, p. 1651
参考文献
Henne; Matuszak
Journal of the American Chemical Society, 1944 , vol. 66, p. 1651