6-硝基-3,4-苯并香豆素合成路线 （共 10 条）
反应条件
indium; ammonium chloride in ethanol; water Reduction; 22 h; Heating;
参考文献
Banik, Bimal K.; Banik, Indrani; Samajdar, Susanta; Wilson, Mary
Heterocycles, 2004 , vol. 63, # 2 p. 283 - 296
反应条件
dipotassium peroxodisulfate; oxygen; silver nitrate in water; acetonitrile
T=50°C; Reagent/catalystSolventTemperatureTime;
参考文献
Wang, Yang; Gulevich, Anton V.; Gevorgyan, Vladimir
Chemistry - A European Journal, 2013 , vol. 19, # 47 p. 15836 - 15840
反应条件
1: potassium tert-butoxide / dimethylsulfoxide / 2 h / 25 °C / Irradiation
2: 59 percent / SiO2 / CH2Cl2 / 24 h / Ambient temperature
View Scheme
参考文献
Petrillo; Novi; Dell'Erva; Tavani
Tetrahedron, 1991 , vol. 47, # 44 p. 9297 - 9304
反应条件
1: potassium tert-butoxide / dimethylsulfoxide / 2 h / 25 °C / Irradiation
2: 59 percent / SiO2 / CH2Cl2 / 24 h / Ambient temperature
View Scheme
参考文献
Petrillo; Novi; Dell'Erva; Tavani
Tetrahedron, 1991 , vol. 47, # 44 p. 9297 - 9304
反应条件
1: bis-triphenylphosphine-palladium(II) chloride; sodium carbonate / tetrahydrofuran; water / 20 - 80 °C / |Schlenk technique; |Inert atmosphere
2: sodium hydroxide; water / tetrahydrofuran / 80 °C
3: dipotassium peroxodisulfate; oxygen; silver nitrate / water; acetonitrile / 50 °C
View Scheme
参考文献
Wang, Yang; Gulevich, Anton V.; Gevorgyan, Vladimir
Chemistry - A European Journal, 2013 , vol. 19, # 47 p. 15836 - 15840
反应条件
1: sodium hydroxide; water / tetrahydrofuran / 80 °C
2: dipotassium peroxodisulfate; oxygen; silver nitrate / water; acetonitrile / 50 °C
View Scheme
参考文献
Wang, Yang; Gulevich, Anton V.; Gevorgyan, Vladimir
Chemistry - A European Journal, 2013 , vol. 19, # 47 p. 15836 - 15840
反应条件
1: bis-triphenylphosphine-palladium(II) chloride; sodium carbonate / tetrahydrofuran; water / 20 - 80 °C / |Schlenk technique; |Inert atmosphere
2: sodium hydroxide; water / tetrahydrofuran / 80 °C
3: dipotassium peroxodisulfate; oxygen; silver nitrate / water; acetonitrile / 50 °C
View Scheme
参考文献
Wang, Yang; Gulevich, Anton V.; Gevorgyan, Vladimir
Chemistry - A European Journal, 2013 , vol. 19, # 47 p. 15836 - 15840
参考文献
Kenner et al.
Tetrahedron, 1957 , vol. 1, p. 259,267
反应条件
nitrogen trioxide
T=22.85°C; Oxidation; P=740 Torr; gas phase; Kinetics; Further Variations:Reagents;
参考文献
Kwok; Harger; Arey; Atkinson
Environmental Science and Technology, 1994 , vol. 28, # 3 p. 521 - 527
反应条件
1: platinum electrodes; aqueous sodium carbonate-solution / Elektrolyse
2: nitric acid
View Scheme
参考文献
Kenner et al.
Tetrahedron, 1957 , vol. 1, p. 259,267
