3-羟基-1,3,3-三苯基-丙-1-酮合成路线 （共 23 条）
反应条件
boron trifluoride diethyl etherate; mercury(II) oxide in tetrahydrofuran; water
Ambient temperature;
参考文献
Stahl, Ingfried; Gosselck, Juergen
Synthesis, 1980 , # 7 p. 561 - 563
反应条件
oxygen in dichloromethane
T=10°C; 6 h; Irradiation; Further byproducts given;
参考文献
Baldovi, Maria V.; Garcia, Hermenegildo; Miranda, Miguel A.; Primo, Jaime
Monatshefte fuer Chemie, 1990 , vol. 121, # 5 p. 371 - 375
反应条件
in acetonitrile
T=15 - 20°C; 5 h; Irradiation; Further byproducts given;
参考文献
Kamata, Masaki; Nishikata, Yasuhiro; Kato, Mitsuaki
Chemical Communications, 1996 , # 21 p. 2407 - 2408
反应条件
mercury(II) p-toluensulfonamidate; water in methanol
T=130°C; P=6000.6 Torr; 27 h; Inert atmosphereMicrowave irradiation; Overall yield = 93 percent; regioselective reaction;
参考文献
Corominas, Albert; Montana, Angel M.
Synthetic Communications, 2013 , vol. 43, # 15 p. 2062 - 2072
参考文献
Landrieu; Blatt
Bulletin de la Societe Chimique de France, 1924 , vol. <4> 35, p. 1429,1430
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Vorlaender; Osterburg; Meye
Chemische Berichte, 1923 , vol. 56, p. 1143
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Clemo; Raper; Robson
Journal of the Chemical Society, 1939 , p. 431,434
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Kohler, Erickson
Journal of the American Chemical Society, 1931 , vol. 53, p. 2301,2307
反应条件
in acetonitrile
T=15 - 20°C; 5 h; Irradiation; Further byproducts given;
参考文献
Kamata, Masaki; Nishikata, Yasuhiro; Kato, Mitsuaki
Chemical Communications, 1996 , # 21 p. 2407 - 2408
反应条件
in acetonitrile
T=15 - 20°C; 5 h; Irradiation; Further byproducts given;
参考文献
Kamata, Masaki; Nishikata, Yasuhiro; Kato, Mitsuaki
Chemical Communications, 1996 , # 21 p. 2407 - 2408
参考文献
Zimmerman; English
Journal of the American Chemical Society, 1954 , vol. 76, p. 2291,2294
反应条件
oxygen in dichloromethane
T=25°C; 24 h; Further byproducts given;
参考文献
Yamamoto, Hiroshi; Miura, Masahiro; Nojima, Masatomo; Kusabayashi, Shigekazu
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 173 - 182
反应条件
1: 1.) Mg / 1.) ether 2.) ether, reflux
2: 70 percent / HgO, BF3*(C2H5)2O / H2O; tetrahydrofuran / Ambient temperature
View Scheme
参考文献
Stahl, Ingfried; Gosselck, Juergen
Synthesis, 1980 , # 7 p. 561 - 563
