3-甲氧基-7,12-二甲基苯并(a)蒽合成路线 （共 8 条）
反应条件
sodium tetrahydroborate in dimethyl sulfoxide
5 h; Ambient temperature;
参考文献
Sukumaran, K.B.; Harvey, Ronald G.
Journal of Organic Chemistry, 1980 , vol. 45, # 22 p. 4407 - 4413
反应条件
methanesulfonic acid in dichloromethane
0.166667 h;
参考文献
Harvey, Ronald G.; Dai, Qing; Ran, Chongzhao; Penning, Trevor M.
Journal of Organic Chemistry, 2004 , vol. 69, # 6 p. 2024 - 2032
反应条件
lithium aluminium tetrahydride; titanium(III) chloride in tetrahydrofuran
2 h; Heating; Yield given;
参考文献
Lee; Harvey
Journal of Organic Chemistry, 1986 , vol. 51, # 18 p. 3502 - 3507
反应条件
methanesulfonic acid in dichloromethane
4 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Lee; Harvey
Journal of Organic Chemistry, 1986 , vol. 51, # 18 p. 3502 - 3507
反应条件
1: BBr3 / CH2Cl2 / 20 °C
2: 0.10 g / o-iodoxybenzoic acid / dimethylformamide / 0.17 h
View Scheme
参考文献
Sukumaran,K.B.; Harvey,R.G.
Journal of the American Chemical Society, 1979 , vol. 101, # 5 p. 1353 - 1354
反应条件
1: BBr3 / CH2Cl2 / 20 °C
2: 0.10 g / o-iodoxybenzoic acid / dimethylformamide / 0.17 h
3: NaBH4 / dimethylformamide
View Scheme
参考文献
Sukumaran, K.B.; Harvey, Ronald G.
Journal of Organic Chemistry, 1980 , vol. 45, # 22 p. 4407 - 4413
反应条件
1: BBr3 / CH2Cl2 / 20 °C
2: 0.10 g / o-iodoxybenzoic acid / dimethylformamide / 0.17 h
3: NaBH4; O2
View Scheme
参考文献
Sukumaran,K.B.; Harvey,R.G.
Journal of the American Chemical Society, 1979 , vol. 101, # 5 p. 1353 - 1354
反应条件
lithium methylmercaptide in N,N-dimethyl-formamide
4 h; Heating;
参考文献
Sukumaran, K.B.; Harvey, Ronald G.
Journal of Organic Chemistry, 1980 , vol. 45, # 22 p. 4407 - 4413
