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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
1-碘-7-甲氧基萘
合成路线
（共 10 条）
66240-21-9
1-碘-7-甲氧基萘
→
反应条件
158365-54-9
7-甲氧基-1-萘并ni三le
反应条件
in 1-methyl-pyrrolidin-2-one T=150°C; Rosenmund-van Braun Cyanation; 2 h;
参考文献
Kandagatla, Bhaskar; Raju, Vetukuri Venkata Naga Kali Vara Prasada; Reddy, Ganta Madhusudhan; Rao, Sirigiri Chandrakanth; Iqbal, Javed; Bandichhor, Rakeshwar; Oruganti, Srinivas
Tetrahedron Letters, 2012 , vol. 53, # 52 p. 7125 - 7127
66240-21-9
1-碘-7-甲氧基萘
→
反应条件
138112-76-2
阿戈美拉汀
反应条件
1.1: n-butyllithium / hexane; tetrahydrofuran / 1.5 h / -78 - 5 °C / |Inert atmosphere 1.2: 0.5 h / -78 °C / |Inert atmosphere 2.1: ammonium acetate / toluene / 14 h / 100 °C 3.1: palladium 10 on activated carbon; acetic acid View Scheme
参考文献
Kandagatla, Bhaskar; Raju, Vetukuri Venkata Naga Kali Vara Prasada; Reddy, Ganta Madhusudhan; Rao, Sirigiri Chandrakanth; Iqbal, Javed; Bandichhor, Rakeshwar; Oruganti, Srinivas
Tetrahedron Letters, 2012 , vol. 53, # 52 p. 7125 - 7127
66240-21-9
1-碘-7-甲氧基萘
→
反应条件
138113-09-4
7-甲氧基-1-萘乙胺
反应条件
1.1: n-butyllithium / hexane; tetrahydrofuran / 1.5 h / -78 - 5 °C / |Inert atmosphere 1.2: 0.5 h / -78 °C / |Inert atmosphere 2.1: ammonium acetate / toluene / 14 h / 100 °C 3.1: palladium 10 on activated carbon; hydrogen / ethanol / 20 °C / 3102.97 Torr View Scheme
参考文献
Kandagatla, Bhaskar; Raju, Vetukuri Venkata Naga Kali Vara Prasada; Reddy, Ganta Madhusudhan; Rao, Sirigiri Chandrakanth; Iqbal, Javed; Bandichhor, Rakeshwar; Oruganti, Srinivas
Tetrahedron Letters, 2012 , vol. 53, # 52 p. 7125 - 7127
66240-21-9
1-碘-7-甲氧基萘
+
68-12-2
N,N-二甲基甲酰胺
→
反应条件
158365-55-0
7-甲氧基萘-1-羧醛
反应条件
1: 1-iodo-7-methoxynaphthalene With n-butyllithium in tetrahydrofuran; hexane T=-78 - 5°C; 1.5 h; Inert atmosphere; 2: N,N-dimethyl-formamide in tetrahydrofuran; hexane T=-78°C; 0.5 h; Inert atmosphere;
参考文献
Kandagatla, Bhaskar; Raju, Vetukuri Venkata Naga Kali Vara Prasada; Reddy, Ganta Madhusudhan; Rao, Sirigiri Chandrakanth; Iqbal, Javed; Bandichhor, Rakeshwar; Oruganti, Srinivas
Tetrahedron Letters, 2012 , vol. 53, # 52 p. 7125 - 7127
66240-21-9
1-碘-7-甲氧基萘
→
反应条件
158365-55-0
7-甲氧基萘-1-羧醛
反应条件
1: 1-methyl-pyrrolidin-2-one / 2 h / 150 °C 2: diisobutylaluminium hydride / dichloromethane; toluene / 2 h / -78 - 45 °C / |Inert atmosphere View Scheme
参考文献
Kandagatla, Bhaskar; Raju, Vetukuri Venkata Naga Kali Vara Prasada; Reddy, Ganta Madhusudhan; Rao, Sirigiri Chandrakanth; Iqbal, Javed; Bandichhor, Rakeshwar; Oruganti, Srinivas
Tetrahedron Letters, 2012 , vol. 53, # 52 p. 7125 - 7127
29921-51-5
8-碘-2-萘酚
+
77-78-1
硫酸二甲酯
→
反应条件
66240-21-9
1-碘-7-甲氧基萘
反应条件
1: 1-iodo-7-hydroxynaphthalene With potassium carbonate in acetone T=20°C; 0.25 h; 2: dimethyl sulfate in acetone T=20°C; 3 h;
参考文献
Kandagatla, Bhaskar; Raju, Vetukuri Venkata Naga Kali Vara Prasada; Reddy, Ganta Madhusudhan; Rao, Sirigiri Chandrakanth; Iqbal, Javed; Bandichhor, Rakeshwar; Oruganti, Srinivas
Tetrahedron Letters, 2012 , vol. 53, # 52 p. 7125 - 7127
5302-79-4
7-甲氧基-1-萘胺
→
反应条件
66240-21-9
1-碘-7-甲氧基萘
反应条件
hydrogenchloride; acetic acid; potassium iodide T=80°C; Diazotization;
参考文献
Bachmann; Horton
Journal of the American Chemical Society, 1947 , vol. 69, p. 58,59
93189-18-5
N-(7-甲氧基萘-1-基)乙酰胺
→
反应条件
66240-21-9
1-碘-7-甲氧基萘
反应条件
1: aqueous hydrochloric acid 2: aqueous HCl; acetic acid; KI / 80 °C / Diazotization View Scheme
参考文献
Bachmann; Horton
Journal of the American Chemical Society, 1947 , vol. 69, p. 58,59
6470-18-4
1-乙酰氨基-7-萘酚
→
反应条件
66240-21-9
1-碘-7-甲氧基萘
反应条件
1: aqueous NaOH-solution 2: aqueous hydrochloric acid 3: aqueous HCl; acetic acid; KI / 80 °C / Diazotization View Scheme
参考文献
Bachmann; Horton
Journal of the American Chemical Society, 1947 , vol. 69, p. 58,59
118-46-7
→
反应条件
66240-21-9
1-碘-7-甲氧基萘
反应条件
1.1: hydrogenchloride; sodium nitrite / water / 1 h / 0 - 5 °C 1.2: 2.5 h / 0 - 5 °C 2.1: potassium carbonate / acetone / 0.25 h / 20 °C 2.2: 3 h / 20 °C View Scheme
参考文献
Kandagatla, Bhaskar; Raju, Vetukuri Venkata Naga Kali Vara Prasada; Reddy, Ganta Madhusudhan; Rao, Sirigiri Chandrakanth; Iqbal, Javed; Bandichhor, Rakeshwar; Oruganti, Srinivas
Tetrahedron Letters, 2012 , vol. 53, # 52 p. 7125 - 7127
