3,8-二甲基-4,6-癸二炔-3,8-二醇合成路线 (共 6 条)
反应条件
copper(l) iodide; N,N,N',N,-tetramethylethylenediamine; oxygen in acetonitrile
T=50°C; Hay Coupling;
参考文献
Wu, Wanqing; Gao, Yang; Jiang, Huanfeng; Huang, Yubing
Journal of Organic Chemistry, 2013 , vol. 78, # 9 p. 4580 - 4586
反应条件
copper(l) chloride in dimethyl sulfoxide
T=80°C; 6 h; Inert atmosphere;
参考文献
Shaibakova; Titova; Ibragimov; Dzhemilev
Russian Journal of Organic Chemistry, 2011 , vol. 47, # 2 p. 161 - 167
反应条件
sodium azide; diethyl ether
参考文献
I.G.Farbenind.
Patent: FR765469 , 1933 ;
反应条件
morpholine in acetone
T=20°C; cross-coupling Glaser reaction; 24 h;
参考文献
Fodor, Anna; Kiss, Arpad; Debreczeni, Nora; Hell, Zoltan; Gresits, Ivan
Organic and Biomolecular Chemistry, 2010 , vol. 8, # 20 p. 4575 - 4581
参考文献
Armitage et al.
Journal of the Chemical Society, 1951 , p. 44,47
Journal of the Chemical Society, 1952 , p. 1993,1996
参考文献
Bowden et al.
Journal of the Chemical Society, 1947 , p. 1582