(S)-1-甲基 3-(p-甲氧基苯基)-丙胺合成路线 (共 4 条)
反应条件
hydrogen; palladium on activated charcoal in ethanol
T=20°C;
参考文献
Chattopadhyay, Sunil K.; Srivastava, Sachin; Sashidhara, Koneni V.; Tripathi, Arun K.; Bhattacharya, Asish K.; Negi, Arvind S.
Bioorganic and Medicinal Chemistry Letters, 2004 , vol. 14, # 7 p. 1729 - 1731
反应条件
1: 70 percent / aq. HBr / 6 h / 80 °C
2: 85 percent / K2CO3 / acetone / 4 h / Heating
3: 80 percent / NaN3 / dimethylformamide / 6 h / 70 °C
4: 80 percent / H2 / Pd/C / ethanol / 20 °C
View Scheme
参考文献
Chattopadhyay, Sunil K.; Srivastava, Sachin; Sashidhara, Koneni V.; Tripathi, Arun K.; Bhattacharya, Asish K.; Negi, Arvind S.
Bioorganic and Medicinal Chemistry Letters, 2004 , vol. 14, # 7 p. 1729 - 1731
反应条件
1: 85 percent / K2CO3 / acetone / 4 h / Heating
2: 80 percent / NaN3 / dimethylformamide / 6 h / 70 °C
3: 80 percent / H2 / Pd/C / ethanol / 20 °C
View Scheme
参考文献
Chattopadhyay, Sunil K.; Srivastava, Sachin; Sashidhara, Koneni V.; Tripathi, Arun K.; Bhattacharya, Asish K.; Negi, Arvind S.
Bioorganic and Medicinal Chemistry Letters, 2004 , vol. 14, # 7 p. 1729 - 1731
反应条件
1: 80 percent / NaN3 / dimethylformamide / 6 h / 70 °C
2: 80 percent / H2 / Pd/C / ethanol / 20 °C
View Scheme
参考文献
Chattopadhyay, Sunil K.; Srivastava, Sachin; Sashidhara, Koneni V.; Tripathi, Arun K.; Bhattacharya, Asish K.; Negi, Arvind S.
Bioorganic and Medicinal Chemistry Letters, 2004 , vol. 14, # 7 p. 1729 - 1731