2-N-丁氧基-5-硝基吡啶合成路线 (共 4 条)
反应条件
hydrogen; palladium on activated charcoal in ethanol P=15201 Torr; 2 h;
参考文献
ASTRAZENECA AB
Patent: WO2008/112440 A1, 2008 ;
Location in patent: Page/Page column 42 ;
WO 2008/112440 A1
反应条件
1: butan-1-ol With sodium hydride in N,N-dimethyl-formamide
T=0°C; 0.0833333 h;
2: 2-chloro-5-nitro-pyridine in N,N-dimethyl-formamide
T=0 - 20°C;
参考文献
ASTRAZENECA AB
Patent: WO2008/112440 A1, 2008 ;
Location in patent: Page/Page column 42 ;
WO 2008/112440 A1
参考文献
Schering-Kahlbaum A.G.
Patent: US1862361 , 1929 ;
Full Text Show Details
Schering-Kahlbaum A.G.
Patent: DE543288 , 1928 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, 17738
反应条件
sulfuric acid; nitric acid
参考文献
Chem. Fabr. v. Heyden
Patent: DE568549 , 1932 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 19, p. 1137