N-烯丙基-n-甲基苯胺合成路线 （共 44 条）
反应条件
aluminium trichloride in xylene T=140°C; 48 h; Further byproducts given;
参考文献
Journal of Organic Chemistry, , vol. 58, # 19 p. 5095 - 5100
反应条件
tetrabutylammomium bromide; sodium acetate; palladium diacetate; triphenylphosphine in N,N-dimethyl-formamide T=120°C; Heck reaction; 8 h; in air;
参考文献
Jiang, Tao-Shan; Li, Jin-Heng
Chemical Communications, 2009 , # 46 p. 7236 - 7238
反应条件
1: With (R,R)-BDPP; benzo[1,3,2]dioxaborole; [RhCl(η2:η2-cycloocta-1,5-diene)]2 in tetrahydrofuran T=25°C; 1 h; 2: With sodium hydroxide; dihydrogen peroxide in tetrahydrofuran; ethanol Further stages.;
参考文献
Lillo, Vanesa; Fernandez, Elena; Segarra, Anna M.
Tetrahedron Asymmetry, 2007 , vol. 18, # 8 p. 911 - 914
反应条件
hydrogenchloride; sodium tetrahydroborate; dihydrogen peroxide; sodium carbonate 1.) ether 2.) THF, reflux, 3h; Yield given. Multistep reaction;
参考文献
Baboulene, Michel; Torregrosa, Jean-Luc; Speziale, Vincent; Lattes, Armand
Bulletin de la Societe Chimique de France, 1980 , vol. 2, # 11-12 p. 565 - 570
反应条件
tetrabutylammomium bromide; sodium acetate; palladium diacetate; triphenylphosphine in N,N-dimethyl-formamide T=120°C; Heck reaction; 10 h; in air;
参考文献
Jiang, Tao-Shan; Li, Jin-Heng
Chemical Communications, 2009 , # 46 p. 7236 - 7238
反应条件
hydrogenchloride; sodium nitrite T=0°C; anschlissendes Kochen mit verduennter Alkalilauge;
参考文献
Zeile; Meyer
Hoppe-Seyler's Zeitschrift fuer Physiologische Chemie, 1939 , vol. 256, p. 137
反应条件
in benzene T=150°C; 20 h;
参考文献
Kobayashi, Yoshiro; Nagai, Takabumi; Kumadaki, Itsumaro
Chemical and Pharmaceutical Bulletin, 1984 , vol. 32, # 12 p. 5031 - 5035
反应条件
1: benzene / 20 h / 150 °C 2: 22.2 percent / benzene / 25 h / 140 °C View Scheme
参考文献
Kobayashi, Yoshiro; Nagai, Takabumi; Kumadaki, Itsumaro
Chemical and Pharmaceutical Bulletin, 1984 , vol. 32, # 12 p. 5031 - 5035
反应条件
tetrabutylammomium bromide; sodium acetate; palladium diacetate; triphenylphosphine in N,N-dimethyl-formamide T=120°C; Heck reaction; 4 h; in air;
参考文献
Jiang, Tao-Shan; Li, Jin-Heng
Chemical Communications, 2009 , # 46 p. 7236 - 7238
反应条件
tetrabutylammomium bromide; sodium acetate; palladium diacetate; triphenylphosphine in N,N-dimethyl-formamide T=100°C; Heck reaction; 14 h; in air;
参考文献
Jiang, Tao-Shan; Li, Jin-Heng
Chemical Communications, 2009 , # 46 p. 7236 - 7238
