N-(1-甲基-2-氧代丙基)乙酰胺合成路线 (共 18 条)
反应条件
hydrogenchloride Destillieren des Reaktionsprodukts mit Quecksilber(II)-chlorid und Kaliumcarbonat;
参考文献
Dakin; West
Journal of Biological Chemistry, 1928 , vol. 78, p. 102
反应条件
beim Destillieren des Reaktionsprodukts mit Quecksilber(II)-chlorid und Kaliumcarbonat;
参考文献
Dakin; West
Journal of Biological Chemistry, 1928 , vol. 78, p. 102
反应条件
ethanethiolic acid; zinc(II) chloride in 1,4-dioxane
参考文献
Takahashi,T.; Hayami,M.
Yakugaku Zasshi, 1961 , vol. 81, p. 1419 - 1426
参考文献
Wiley; Borum
Journal of the American Chemical Society, 1948 , vol. 70, p. 2006
参考文献
Wiley; Borum
Journal of the American Chemical Society, 1948 , vol. 70, p. 2006
反应条件
sodium hydroxide in methanol 1.) 0 deg C, 15 min, pH 10, 2.) 60-65 deg C, 30 min, pH 9-10;
参考文献
Bayomi; Al-Obaid; Jado; Loutfy
Indian Journal of Chemistry - Section B Organic Chemistry Including Medicinal Chemistry, 1990 , vol. 29, # 1 p. 47 - 52
反应条件
hydrogen; palladium on activated charcoal in ethanol
7 h;
参考文献
Atkinson, Robert S.; Edwards, Paul J.; Thomson, Gordon A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 21 p. 3209 - 3216
参考文献
Yuan; Chen
Synthesis, 1992 , # 6 p. 531 - 532
反应条件
formic acid; 4-methyl-N-((1R,2R)-2-{[(4-methylphenyl)sulfonyl]amino}-1,2-diphenylethyl)benzenesulfonamide; triethylamine; [Ru2(p-PriC6H4Me)2(μ-Cl)Cl]2
T=28°C; 48 h;
参考文献
Peach, Philip; Cross, David J.; Kenny, Jennifer A.; Mann, Inderjit; Houson, Ian; Campbell, Lynne; Walsgrove, Tim; Wills, Martin
Tetrahedron, 2006 , vol. 62, # 8 p. 1864 - 1876
反应条件
1: 95 percent / ethyl acetate / 0.02 h / Heating
2: allyltrimethylsilane, boron trifluoride-diethyl ether / tetrahydrofuran
3: 89 percent / H2 / palladium on charcoal / ethanol / 7 h
View Scheme
参考文献
Atkinson, Robert S.; Edwards, Paul J.; Thomson, Gordon A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 21 p. 3209 - 3216