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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4,5-二氢芘
合成路线
（共 42 条）
129-00-0
芘
→
反应条件
6628-98-4
4,5-二氢芘
+
781-17-9
4,5,9,10-四氢苯芘
+
1732-13-4
1,2,3,6,7,8-六氢芘
+
55821-21-1
+
5385-37-5
1,2,3a,3,4,5-六氢芘
+
14698-02-3
1,2,3,3A,4,5,5A,6,7,8-十氢芘
反应条件
hydrogen in decane T=249.84°C; P=46504.7 Torr; 1.33333 h; Autoclave; KineticsEquilibrium constant; Reagent/catalyst; chemoselective reaction;
参考文献
Lin, Qiang; Shimizu, Ken-Ichi; Satsuma, Atsushi
Applied Catalysis A: General, 2010 , vol. 387, # 1-2 p. 166 - 172
51744-98-0
→
反应条件
129-00-0
芘
+
6628-98-4
4,5-二氢芘
+
781-17-9
4,5,9,10-四氢苯芘
+
55775-16-1
+
5385-37-5
1,2,3a,3,4,5-六氢芘
+
53076-44-1
反应条件
hydrogenchloride; aluminium trichloride in carbon disulfide Heating; Product distribution;
参考文献
Sato, Takeo; Nishiyama, Kozaburo; Morita, Akira; Iitaka, Yoichi
Bulletin of the Chemical Society of Japan, 1985 , vol. 58, # 8 p. 2366 - 2369
7647-01-0
盐酸
→
反应条件
6628-98-4
4,5-二氢芘
反应条件
暂无反应条件数据
参考文献
Newman; Whitehouse
Journal of the American Chemical Society, 1949 , vol. 71, p. 3664,3666
6628-98-4
4,5-二氢芘
→
反应条件
82799-67-5
反应条件
1: 95 percent / Li / tetrahydrofuran; liquid ammonia / 0.03 h / -78 °C / further reducing agent 2: 94 percent / AlCl3 / CS2 / 2 h / Ambient temperature View Scheme
参考文献
Harvey, Ronald G.; Konieczny, Maria; Pataki, John
Journal of Organic Chemistry, 1983 , vol. 48, # 17 p. 2930 - 2932
6628-98-4
4,5-二氢芘
→
反应条件
86470-96-4
反应条件
1: H2 / 10percent Pd on charcoal / ethyl acetate / 72 h / 2844.3 Torr 2: 86 percent / 1.) AlCl3, 2.) ice / CS2 / 1.) 0 deg C then RT 2 h 3: 93 percent / 2,3-dichloro-5,6-dicyano-1,4-benzoquinone / benzene / 20 h / Heating 4: NaBH4 / methanol / 2 h 5: 79 percent / p-toluenesulfonic acid / benzene / 20 h / Heating 6: 63 percent / m-chloroperbenzoic acid / tetrahydrofuran / 5 h View Scheme
参考文献
Harvey, Ronald G.; Konieczny, Maria; Pataki, John
Journal of Organic Chemistry, 1983 , vol. 48, # 17 p. 2930 - 2932
6628-98-4
4,5-二氢芘
→
反应条件
86470-97-5
反应条件
1: H2 / 10percent Pd on charcoal / ethyl acetate / 72 h / 2844.3 Torr 2: 98 percent / 1.) AlCl3, 2.) ice / CH2Cl2 / 1.) 0 deg C then RT 2 h 3: 98 percent / 2,3-dichloro-5,6-dicyano-1,4-benzoquinone / benzene / 72 h / Heating 4: 98 percent / NaBH4 / methanol / 2 h 5: 79 percent / p-toluenesulfonic acid / benzene / 20 h / Heating 6: 73 percent / m-chloroperbenzoic acid / CH2Cl2 / 360 h / 4 °C / phosphate buffer (pH 8) View Scheme
参考文献
Harvey, Ronald G.; Konieczny, Maria; Pataki, John
Journal of Organic Chemistry, 1983 , vol. 48, # 17 p. 2930 - 2932
6628-98-4
4,5-二氢芘
→
反应条件
86470-98-6
反应条件
1: H2 / 10percent Pd on charcoal / ethyl acetate / 72 h / 2844.3 Torr 2: 98 percent / 1.) AlCl3, 2.) ice / CH2Cl2 / 1.) 0 deg C then RT 2 h View Scheme
参考文献
Harvey, Ronald G.; Konieczny, Maria; Pataki, John
Journal of Organic Chemistry, 1983 , vol. 48, # 17 p. 2930 - 2932
6628-98-4
4,5-二氢芘
→
反应条件
86470-99-7
alpha-甲基-2-芘甲醇
反应条件
1: H2 / 10percent Pd on charcoal / ethyl acetate / 72 h / 2844.3 Torr 2: 86 percent / 1.) AlCl3, 2.) ice / CS2 / 1.) 0 deg C then RT 2 h 3: 93 percent / 2,3-dichloro-5,6-dicyano-1,4-benzoquinone / benzene / 20 h / Heating 4: NaBH4 / methanol / 2 h View Scheme
参考文献
Harvey, Ronald G.; Konieczny, Maria; Pataki, John
Journal of Organic Chemistry, 1983 , vol. 48, # 17 p. 2930 - 2932
6628-98-4
4,5-二氢芘
→
反应条件
86471-00-3
反应条件
1: H2 / 10percent Pd on charcoal / ethyl acetate / 72 h / 2844.3 Torr 2: 86 percent / 1.) AlCl3, 2.) ice / CS2 / 1.) 0 deg C then RT 2 h 3: 93 percent / 2,3-dichloro-5,6-dicyano-1,4-benzoquinone / benzene / 20 h / Heating 4: NaBH4 / methanol / 2 h 5: 79 percent / p-toluenesulfonic acid / benzene / 20 h / Heating View Scheme
参考文献
Harvey, Ronald G.; Konieczny, Maria; Pataki, John
Journal of Organic Chemistry, 1983 , vol. 48, # 17 p. 2930 - 2932
6628-98-4
4,5-二氢芘
→
反应条件
86471-02-5
反应条件
1: H2 / 10percent Pd on charcoal / ethyl acetate / 72 h / 2844.3 Torr 2: 98 percent / 1.) AlCl3, 2.) ice / CH2Cl2 / 1.) 0 deg C then RT 2 h 3: 98 percent / 2,3-dichloro-5,6-dicyano-1,4-benzoquinone / benzene / 72 h / Heating 4: 98 percent / NaBH4 / methanol / 2 h View Scheme
参考文献
Harvey, Ronald G.; Konieczny, Maria; Pataki, John
Journal of Organic Chemistry, 1983 , vol. 48, # 17 p. 2930 - 2932
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