反应条件
1: iodobenzene With n-butyllithium in tetrahydrofuran; hexane
T=-78°C; 0.5 h; Inert atmosphere;
2: With zinc dibromide in tetrahydrofuran; hexane
T=-78 - 0°C; 0.5 h; Inert atmosphere;
3: trans-1-iodo-1-decene With [Pd{bis[2-(diphenylphosphino)phenyl] ether}Cl2] in tetrahydrofuran; hexane
24 h; RefluxInert atmosphere;
参考文献
Xu, Shiqing; Truex, Nicholas L.; Mohan, Swathi; Negishi, Ei-Ichi
Arkivoc, 2012 , vol. 2012, # 7 p. 242 - 252