反应条件
1: methyl 2-(acetylamino)-2-(dimethylphosphoryl) acetate With N,N,N',N'-tetramethylguanidine in tetrahydrofuran
T=-78°C; 0.25 h;
2: isobutyraldehyde in tetrahydrofuran
T=-78 - 25°C; 2.5 h;
参考文献
Davies, Stephen G.; Rodriguez-Solla, Humberto; Tamayo, Juan A.; Cowley, Andrew R.; Concellon, Carmen; Garner, A. Christopher; Parkes, Alastair L.; Smith, Andrew D.
Organic and Biomolecular Chemistry, 2005 , vol. 3, # 8 p. 1435 - 1447
