1: (methoxymethyl)-triphenylphosphonium chloride With potassium tert-butylate in tetrahydrofuran
T=0°C; 0.5 h;
2: ortho-bromobenzaldehyde in tetrahydrofuran
T=20°C; 12 h;
3: With formic acid in dichloromethane
T=20°C; 72 h; Further stages.;
参考文献
Pedrosa; Andres; Iglesias
Journal of Organic Chemistry, 2001 , vol. 66, # 1 p. 243 - 250
Smithkline Beckman Corporation
Patent: US4874792 A1, 1989 ;
US 4874792 A
Title/Abstract Full Text Show Details
SmithKline Beckman Corporation
Patent: US4820719 A1, 1989 ;
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反应条件
copper monoiodide in triethylamine
参考文献
SmithKline Beecham Corporation
Patent: US4937253 A1, 1990 ;
US 4937253 A