in tetrahydrofuran
dry oxygen-free solvents; sealing mixt. of Ge-compd. in THF and HgCl2 in glass ampoule, heating to 100°C (5 h); Ge(CF3)3Cl not isolated; detn. by (19)F-NMR spectroscopy;
参考文献
Ermolaev, N. L.; Bochkarev, M. N.; Razuvaev, G. A.; Grishin, Yu. K.; Ustynyuk, Yu. A.
Journal of General Chemistry USSR (English Translation), 1984 , vol. 54, p. 83 - 86
Zhurnal Obshchei Khimii, 1984 , vol. 54, p. 96 - 100
hydrogenchloride in benzene
dry oxygen-free solvents; sealing mixt. of Ge-compd. in benzene and HCl in glass ampoule, heating to 100°C (5 h); (CF3)3GeCl and (CF3)3GeH not isolated; detn. by (19)F-NMR spectroscopy;
参考文献
Ermolaev, N. L.; Bochkarev, M. N.; Razuvaev, G. A.; Grishin, Yu. K.; Ustynyuk, Yu. A.
Journal of General Chemistry USSR (English Translation), 1984 , vol. 54, p. 83 - 86
Zhurnal Obshchei Khimii, 1984 , vol. 54, p. 96 - 100