CD3I; dimethyl zinc in neat (no solvent)
byproducts: (CF3)2GeH(CD3), (CF3)2Ge(CH3)(CD3), (CF3)2Ge(CD3)2; Me2Zn and CD3I condensed with (CF3)2GeH2, mixt. warmed to room temp.; fractional condensation;
参考文献
Eujen, R.; Mellies, R.; Petrauskas, E.
Journal of Organometallic Chemistry, 1986 , vol. 299, p. 29 - 40