N-(6-氯-4-甲基-3-吡啶)乙酰胺合成路线 (共 4 条)
反应条件
Yield given. Multistep reaction;
参考文献
Chapman, David; Hurst, Jim
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2398 - 2404
反应条件
potassium acetate; sodium carbonate; nitrosyl chloride 1.) acetic anhydride, acetic acid, 30 min, 2.) benzene, 2 h, reflux; Yield given. Multistep reaction;
参考文献
Chapman, David; Hurst, Jim
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2398 - 2404
反应条件
1: tin(II) chloride, conc. hydrochloric acid / diethyl ether / Heating
2: 5.2 g / toluene / 2 h / 100 °C
View Scheme
参考文献
Chapman, David; Hurst, Jim
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2398 - 2404
反应条件
in toluene
T=100°C; 2 h;
参考文献
Chapman, David; Hurst, Jim
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2398 - 2404