2-(((5-二甲基氨基)甲基)-2-呋喃基)甲基)硫代乙胺合成路线 （共 29 条）
反应条件
hydrogenchloride; hydroquinone T=0°C; 20 h;
参考文献
Navarro; Almeida; Anaya; Moran; Grande; Caballero; Palacios; Montero; San Roman
Pharmazie, 1995 , vol. 50, # 1 p. 12 - 15
反应条件
sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride in acetonitrile 5 h; Ambient temperature;
参考文献
Chachula, Stanislaw; Grynkiewicz, Grzegorz; Szczycinski, Bohdan
Polish Journal of Chemistry, 1990 , vol. 64, # 7 p. 619 - 622
反应条件
sodium hydroxide in water 2 h; Reflux;
参考文献
Mascal, Mark; Dutta, Saikat
Green Chemistry, 2011 , vol. 13, # 11 p. 3101 - 3102
反应条件
1: 91.5 percent / aq. sodium thiosulfate, NaOH / 1 h / 30 °C 2: 65 percent / 50percent aq. NaOH / triethylbenzylammonium chloride / acetonitrile / 5 h / Ambient temperature View Scheme
参考文献
Polish Journal of Chemistry, , vol. 64, # 7 p. 619 - 622
反应条件
1: 70 percent / ethanol / 10 h / Heating 2: 72 percent / conc. HCl, hydroquinone / 20 h / 0 °C View Scheme
参考文献
Pharmazie, , vol. 50, # 1 p. 12 - 15
反应条件
1.1: sodium hydride / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere 1.2: 20 °C / Inert atmosphere 2.1: methanol / 1 h / 20 °C 2.2: 0.58 h / 0 - 20 °C 3.1: sodium hydroxide / water / 2 h / Reflux View Scheme
参考文献
Green Chemistry, , vol. 13, # 11 p. 3101 - 3102
反应条件
1.1: methanol / 1 h / 20 °C 1.2: 0.58 h / 0 - 20 °C 2.1: sodium hydroxide / water / 2 h / Reflux View Scheme
参考文献
Green Chemistry, , vol. 13, # 11 p. 3101 - 3102
反应条件
hydrogenchloride 1.) from 50 to 60 deg C, 2 h, 2.) RT, 16 h; Yield given. Multistep reaction;
参考文献
Polish Journal of Chemistry, , vol. 64, # 7 p. 619 - 622
反应条件
sodium hydroxide in water 4 h; Heating;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 951 - 954
反应条件
1: 90 percent / Na2CO3 / acetonitrile / Ambient temperature 2: 69 percent / Na2CO3 / acetonitrile / Heating View Scheme
参考文献
Valli, Matthew J.; Tang, Yunzhao; Kosh, J. W.; Chapman, James M.; Sowell, J. Walter
Journal of Medicinal Chemistry, 1992 , vol. 35, # 17 p. 3141 - 3147
