2-(((5-二甲基氨基)甲基)-2-呋喃基)甲基)硫代乙胺合成路线 (共 29 条)
反应条件
1: 90 percent / Na2CO3 / acetonitrile / Ambient temperature 2: 41 percent / Na2CO3 / acetonitrile / Heating View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 35, # 17 p. 3141 - 3147
反应条件
1: 90 percent / Na2CO3 / acetonitrile / Ambient temperature 2: 29 percent / NH2NH2, Na2CO3 / acetonitrile / Heating View Scheme
参考文献
Valli, Matthew J.; Tang, Yunzhao; Kosh, J. W.; Chapman, James M.; Sowell, J. Walter
Journal of Medicinal Chemistry, 1992 , vol. 35, # 17 p. 3141 - 3147
反应条件
1: 90 percent / Na2CO3 / acetonitrile / Ambient temperature 2: 95 percent / ammonia, Na2CO3 / acetonitrile / Heating View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 35, # 17 p. 3141 - 3147
反应条件
sodium carbonate in acetonitrile Ambient temperature;
参考文献
Valli, Matthew J.; Tang, Yunzhao; Kosh, J. W.; Chapman, James M.; Sowell, J. Walter
Journal of Medicinal Chemistry, 1992 , vol. 35, # 17 p. 3141 - 3147
反应条件
1: 90 percent / Na2CO3 / acetonitrile / Ambient temperature 2: 41 percent / Na2CO3 / acetonitrile / Heating View Scheme
参考文献
Valli, Matthew J.; Tang, Yunzhao; Kosh, J. W.; Chapman, James M.; Sowell, J. Walter
Journal of Medicinal Chemistry, 1992 , vol. 35, # 17 p. 3141 - 3147
反应条件
1: 90 percent / Na2CO3 / acetonitrile / Ambient temperature 2: 73 percent / Na2CO3 / acetonitrile / Heating View Scheme
参考文献
Valli, Matthew J.; Tang, Yunzhao; Kosh, J. W.; Chapman, James M.; Sowell, J. Walter
Journal of Medicinal Chemistry, 1992 , vol. 35, # 17 p. 3141 - 3147
反应条件
in methanol; methanolic methylamine; acetonitrile
参考文献
Allen and Hanburys Limited
Patent: US4128658 A1, 1978 ;
反应条件
in water T=40°C; 10 h;
参考文献
COUNCIL OF SCIENTIFIC AND INDUSTRIAL RESEARCH
Patent: US2004/186316 A1, 2004 ;
Location in patent: Page 3 ;
反应条件
triethylamine in acetonitrile
Ambient temperature;
参考文献
Sowell Sr.; Tang; Valli; Chapman Jr.; Usher; Vaughan; Kosh
Journal of Medicinal Chemistry, 1992 , vol. 35, # 6 p. 1102 - 1108
反应条件
in pyridine
4 h; Heating;
参考文献
Borchers; Postius; Szelenyi; Schunack
Arzneimittel-Forschung/Drug Research, 1984 , vol. 34, # 7 p. 751 - 754