二甲基二(1-甲基乙基)-锡烷合成路线 （共 3 条）
反应条件
in tetrahydrofuran
boiling, 22h;;
参考文献
Seyferth
Journal of Organic Chemistry, 1957 , vol. 22, p. 1599
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Gmelin Handbook: Sn: Org.Verb.3, 1.1.3.1, page 1 - 24
参考文献
Manghan, J. R.
Patent: US3095433 , 1963 ;
C. A., 1963 , vol. 59, p. 6440
反应条件
in tetrahydrofuran; diethyl ether
(inert atmosphere); addn. of iPrMgCl in THF at 0°C to Me2SnCl2 inEt2O, solvent removal (0°C/13 Torr), reflux (1.5 h); centrifugation at 25°C, washing (petroleum ether), solvent removal (25°C/13 Torr), fractional distn. in vacuo;
参考文献
Appel, Andrea; Kober, Christian; Neumann, Christine; Noeth, Heinrich; Schmidt, Martin; Storch, Wolfgang
Chemische Berichte, 1996 , vol. 129, # 2 p. 175 - 189
