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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
6637-10-1
合成路线
（共 26 条）
120-72-9
吲哚
+
180910-53-6
→
反应条件
27393-85-7
+
6637-10-1
+
58635-45-3
反应条件
formic acid T=20°C; Further byproducts given;
参考文献
Somei, Masanori; Yamada, Fumio; Hayashi, Toshikatsu; Goto, Aya; Saga, Yoshitomo
Heterocycles, 2001 , vol. 55, # 3 p. 457 - 460
120-72-9
吲哚
+
2497-21-4
4-己烯-3-酮
→
反应条件
反应条件
1: indole With Benzoic acid (S)-1-[(S)-5-oxo-2-phenyl-3-(toluene-4-sulfonyl)-[1,3,2]oxazaborolidin-4-yl]-ethyl ester in diethyl ether T=-85°C; Friedel Crafts alkylation; 24 h; Inert atmosphere; 2: hex-4-en-3-one With diethyl ether T=-85°C; Friedel Crafts alkylation; 20 h; Inert atmosphere; optical yield given as percent eeenantioselective reaction;
参考文献
Adachi, Shinya; Tanaka, Fumi; Watanabe, Kazuya; Watada, Atsushi; Harada, Toshiro
Synthesis, 2010 , # 15 art. no. Z12810SS, p. 2652 - 2669
120-72-9
吲哚
+
35356-70-8
2-乙酰胺基丙烯酸甲酯
→
反应条件
6637-10-1
+
2824-57-9
N-乙酰-L-色氨酸甲酯
反应条件
tin(IV) chloride; (R)-3,3'-dibromo-[1,1'-binaphthalene]-2,2'-diol in dichloromethane T=20°C; 2 h; Inert atmosphereMolecular sieve; optical yield given as percent ee;
参考文献
Kieffer, Madeleine E.; Repka, Lindsay M.; Reisman, Sarah E.
Journal of the American Chemical Society, 2012 , vol. 134, # 11 p. 5131 - 5137
122709-55-1
→
反应条件
6637-10-1
反应条件
1: 1N HCl / 0.5 h 2: POCl3 / acetonitrile / 0.25 h / Heating View Scheme
参考文献
Frost, Jonatan R.; Gaudilliere, Bernard R. P.; Kauffmann, Elisabeth; Loyaux, Denis; Normand, Nadine; at al.
Heterocycles, 1989 , vol. 28, # 1 p. 175 - 182
120-72-9
吲哚
+
1016-47-3
N-乙酰基色胺
→
反应条件
6637-10-1
+
122709-57-3
+
122709-55-1
反应条件
trichlorophosphate in acetonitrile 0.25 h; Heating; Further byproducts given. Yields of byproduct given;
参考文献
Frost, Jonatan R.; Gaudilliere, Bernard R. P.; Kauffmann, Elisabeth; Loyaux, Denis; Normand, Nadine; at al.
Heterocycles, 1989 , vol. 28, # 1 p. 175 - 182
120-72-9
吲哚
+
158723-45-6
→
反应条件
6637-10-1
反应条件
methanol; acetyl chloride Addition; dimerization; Title compound not separated from byproducts;
参考文献
Chalaye-Mauger, Helene; Denis, Jean-Noel; Averbuch-Pouchot, Marie-Therese; Vallee, Yannick
Tetrahedron, 2000 , vol. 56, # 5 p. 791 - 804
120-72-9
吲哚
→
反应条件
27393-85-7
+
6637-10-1
+
6941-73-7
2-[2,2-双-(1H-吲哚-3-基)-乙基]-苯胺
反应条件
formic acid; N,N-dimethyl-1-hydroxyindole-3-acetamide T=20°C; 2 h; Product distribution; Further Variations:ReagentsSolvents;
参考文献
Yamada, Fumio; Goto, Aya; Peng, Wu; Hayashi, Toshikatsu; Saga, Yoshitomo; Somei, Masanori
Heterocycles, 2003 , vol. 61, p. 163 - 172
120-72-9
吲哚
+
1484-27-1
→
反应条件
6637-10-1
反应条件
trifluoroacetic acid 1.) room temp., 1 h, dichloromethanemp; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given;
参考文献
Bocchi Vittorio; Palla Gerardo
Tetrahedron, 1986 , vol. 42, # 18 p. 5019 - 5024
120-72-9
吲哚
+
7647-01-0
盐酸
+
71-43-2
苯
→
反应条件
6637-10-1
反应条件
暂无反应条件数据
参考文献
Smith
Chemistry and Industry (London, United Kingdom), 1954 , p. 1451
Full Text Show Details
Hodson; Smith
Journal of the Chemical Society, 1957 , p. 3544
6637-10-1
→
反应条件
111296-91-4
反应条件
1: palladium on activated charcoal / toluene / 3 h / 111 °C 2: acetic acid / 8 h / 118 °C / Inert atmosphere View Scheme
参考文献
Nippon Steel Chemical Co., Ltd.
Patent: EP2415772 A1, 2012 ;
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