5-乙基-2-苯基-4,5-二氢-1,3-噻唑合成路线 (共 6 条)
反应条件
toluene-4-sulfonic acid in toluene
20 h; Heating;
参考文献
Engman, Lars
Journal of Organic Chemistry, 1991 , vol. 56, # 10 p. 3425 - 3430
反应条件
triphenylstannane; 2,2'-azo-bisisobutyronitrile
2 h;
参考文献
Engman, Lars
Journal of Organic Chemistry, 1991 , vol. 56, # 10 p. 3425 - 3430
反应条件
1: 82 percent / Lawesson's reagent / tetrahydrofuran / Heating
2: CHCl3 / 3 h
3: 83 percent / Ph3SnH / AIBN / 2 h
View Scheme
参考文献
Engman, Lars
Journal of Organic Chemistry, 1991 , vol. 56, # 10 p. 3425 - 3430
反应条件
tetraphosphorus decasulfide in toluene
Heating;
参考文献
Smith,P.A.S.; Sullivan,J.M.
Journal of Organic Chemistry, 1961 , vol. 26, p. 1132 - 1136
反应条件
aluminium trichloride in nitrobenzene
参考文献
Smith,P.A.S.; Sullivan,J.M.
Journal of Organic Chemistry, 1961 , vol. 26, p. 1132 - 1136
反应条件
1: K2CO3
2: P2S5 / toluene / Heating
View Scheme
参考文献
Smith,P.A.S.; Sullivan,J.M.
Journal of Organic Chemistry, 1961 , vol. 26, p. 1132 - 1136