4,5-二甲基-2-苯基-1,3,2-二氧硼戊环合成路线 (共 25 条)
反应条件
NiCl2((PPh3)P)2; n-butyllithium 1.) THF, hexane, 0 deg C, 15 min, 2.) THF, hexane, 13 h, 60 deg C; Yield given. Multistep reaction;
参考文献
Kobayashi, Yuichi; Mizojiri, Ryo
Tetrahedron Letters, 1996 , vol. 37, # 47 p. 8531 - 8534
参考文献
Bowie,R.A.; Musgrave,O.C.
Journal of the Chemical Society, 1963 , p. 3945 - 3949
参考文献
Batrakov,S.G. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1974 , vol. 23, p. 1662 - 1668
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1974 , vol. 23, p. 1739 - 1747
反应条件
n-butyllithium; 1,1'-bis(diphenylphosphanyl)ferrocenenickel(II) chloride; potassium iodide in tetrahydrofuran; hexane
T=60°C; Arylation;
参考文献
Kobayashi, Yuichi; Ito, Michiko
European Journal of Organic Chemistry, 2000 , # 20 p. 3393 - 3397
反应条件
n-butyllithium; 1,1'-bis(diphenylphosphanyl)ferrocenenickel(II) chloride; potassium iodide in tetrahydrofuran; hexane
T=60°C; Arylation;
参考文献
Kobayashi, Yuichi; Ito, Michiko
European Journal of Organic Chemistry, 2000 , # 20 p. 3393 - 3397