1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine in dichloromethane T=0°C; 12 h; Inert atmosphere;
参考文献
Duong, Hung A.; Gilligan, Ruth E.; Cooke, Michael L.; Phipps, Robert J.; Gaunt, Matthew J.
Angewandte Chemie - International Edition, 2011 , vol. 50, # 2 p. 463 - 466
1: (3-methoxy-phenyl)-acetic acid With 1,1'-carbonyldiimidazole in dichloromethane T=20°C; 2: O,N-dimethyl-hydroxylamine hydrochloride in dichloromethane T=20°C;