2-甲基-喹喔啉 1,4-二氧化物合成路线 （共 23 条）
反应条件
1: benzene; SeO2 2: aqueous H2O2; acetic acid; acetic acid anhydride View Scheme
参考文献
Elina; Magidson
Zhurnal Obshchei Khimii, 1955 , vol. 25, p. 161,163; engl. Ausg. S. 145, 147
反应条件
bromine in ethyl acetate 2.5 h; Heating;
参考文献
Haddadin, Makhluf J.; Kattan, Asma M. A.; Issidorides, Costas H.
Journal of Organic Chemistry, 1985 , vol. 50, # 1 p. 129 - 130
反应条件
T=185 - 190°C; 0.333333 h; Product distribution;
参考文献
Journal of Heterocyclic Chemistry, , vol. 24, p. 949 - 953
反应条件
1: 55 percent / Br2 / ethyl acetate / 2.5 h / Heating 2: 56 percent / silver nitrate / acetonitrile / 1.5 h / Ambient temperature 3: 96 percent / CH2Cl2 View Scheme
参考文献
Haddadin, Makhluf J.; Kattan, Asma M. A.; Issidorides, Costas H.
Journal of Organic Chemistry, 1985 , vol. 50, # 1 p. 129 - 130
反应条件
T=185 - 190°C; 0.333333 h; Product distribution;
参考文献
Journal of Heterocyclic Chemistry, , vol. 24, p. 949 - 953
反应条件
HOF* CH3CN in chloroform
T=0°C; 0.0333333 h;
参考文献
Carmeli, Mira; Rozen, Shlomo
Journal of Organic Chemistry, 2006 , vol. 71, # 15 p. 5761 - 5765
反应条件
in acetone; acetonitrile
参考文献
Research Corporation
Patent: US4343942 A1, 1982 ;
反应条件
ammonium hydroxide in acetone
参考文献
Research Corporation
Patent: US4343942 A1, 1982 ;
反应条件
caesium carbonate in tetrahydrofuran
T=60°C; 48 h;
参考文献
Dahbi, Samir; Methnani, Ebtissem; Bisseret, Philippe
Tetrahedron Letters, 2010 , vol. 51, # 42 p. 5516 - 5520
反应条件
1: benzofurazan-1-oxide With β-cyclodextrin in methanol; water
Beirut reaction; 0.5 h;
2: propionaldehyde in methanol; water
T=20°C; Beirut reaction; 0.416667 h;
参考文献
Sun, Tao; Zhao, Wen-Jing; Hao, Ai-You; Sun, Li-Zhen
Synthetic Communications, 2011 , vol. 41, # 20 p. 3097 - 3105
