(9CI)-1-乙酰基-1,2,3,4-四氢喹噁啉合成路线 （共 4 条）
反应条件
1: With ozone in methanol
T=-78°C;
2: With hydrogen; nitrobenzene; palladium on activated charcoal in methanol
T=25°C; P=3040 Torr;
参考文献
Bunce, Richard A.; Herron, Derrick M.; Hale, Lu Y.
Journal of Heterocyclic Chemistry, 2003 , vol. 40, # 6 p. 1031 - 1039
参考文献
Morley
Journal of the Chemical Society, 1952 , p. 4008,4012
反应条件
acetic anhydride in ethanol; water
参考文献
Minnesota Mining and Manufacturing Company
Patent: US4348521 A1, 1982 ;
反应条件
1.1: 85 percent / NaH / dimethylformamide / 8.5 h / 20 °C
2.1: O3 / methanol / -78 °C
2.2: 64 percent / H2; nitrobenzene / Pd/C / methanol / 25 °C / 3040 Torr
View Scheme
参考文献
Bunce, Richard A.; Herron, Derrick M.; Hale, Lu Y.
Journal of Heterocyclic Chemistry, 2003 , vol. 40, # 6 p. 1031 - 1039
