反应条件
1.1: palladium diacetate; PCy3∙HBF4; potassium carbonate / dimethyl sulfoxide / 0.17 h / 140 °C / 10343.2 Torr / |Microwave irradiation
2.1: hydrogen bromide / 0.5 h / 10 °C
2.2: 2 h / 20 °C
3.1: Dess-Martin periodane / dichloromethane / 0.25 h / 20 °C
4.1: sodium tris(acetoxy)borohydride / tetrahydrofuran; dichloromethane / 2 h / 0 - 20 °C
View Scheme
参考文献
Kapadia, Nirav; Harding, Wayne
Tetrahedron, 2013 , vol. 69, # 42 p. 8914 - 8920
